C₂₇H₃₉N₇OSSi

Base Information

Chemical Name:C₂₇H₃₉N₇OSSi
CAS No.:1094071-89-2
Molecular Formula:C₂₇H₃₉N₇OSSi
Molecular Weight:537.804
Hs Code.:

C<sub>27</sub>H<sub>39</sub>N<sub>7</sub>OSSi

Synonyms:C₂₇H₃₉N₇OSSi

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Chemical Property of C₂₇H₃₉N₇OSSi

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Technology Process of C₂₇H₃₉N₇OSSi

There total 8 articles about C₂₇H₃₉N₇OSSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1094070-83-3
C₂₇H₃₇N₇O₂SSi

: 1094071-89-2
C₂₇H₃₉N₇OSSi

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; dichloromethane; at 20 - 40 ℃; for 5.16667h;

Reference yield:

: 1094070-82-2
C₂₁H₂₆N₆O₃SSi

: 1094071-89-2
C₂₇H₃₉N₇OSSi

Guidance literature:: Multi-step reaction with 2 steps

1: 4-methyl-morpholine; HATU / N,N-dimethyl-formamide / 16 h / 20 °C

2: lithium aluminium tetrahydride / diethyl ether; dichloromethane / 5.17 h / 20 - 40 °C

With 4-methyl-morpholine; lithium aluminium tetrahydride; HATU; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 192879-33-7
methyl 5-aminothiophene-3-carboxylate

: 1094071-89-2
C₂₇H₃₉N₇OSSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 20 °C

1.2: 0.17 h

2.1: sodium hydroxide; water / tetrahydrofuran; methanol / 16 h / 20 °C

2.2: pH 3 - 4

3.1: 4-methyl-morpholine; HATU / N,N-dimethyl-formamide / 16 h / 20 °C

4.1: lithium aluminium tetrahydride / diethyl ether; dichloromethane / 5.17 h / 20 - 40 °C

With 4-methyl-morpholine; sodium hydroxide; lithium aluminium tetrahydride; water; sodium hydride; HATU; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;