Technology Process of C2HF3O2*C30H32Cl2FN3O4
There total 6 articles about C2HF3O2*C30H32Cl2FN3O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C31H34Cl2FN3O4;
With
lithium hydroxide monohydrate; water;
In
tetrahydrofuran;
for 2h;
trifluoroacetic acid;
In
tetrahydrofuran; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: water; lithium hydroxide monohydrate / tetrahydrofuran / 2 h
2: dmap; N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 20 °C
3: water; lithium hydroxide monohydrate / tetrahydrofuran / 2 h
With
dmap; lithium hydroxide monohydrate; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: piperidine / methanol
2: toluene; tetrahydrofuran / 3 h / Reflux
3: sulfuric acid / 5 h / 50 °C
4: water; cerium(IV)diammonium nitrate / acetonitrile; tetrahydrofuran / 0.25 h
5: water; lithium hydroxide monohydrate / tetrahydrofuran / 2 h
6: dmap; N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 20 °C
7: water; lithium hydroxide monohydrate / tetrahydrofuran / 2 h
With
piperidine; dmap; cerium(IV)diammonium nitrate; lithium hydroxide monohydrate; sulfuric acid; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; methanol; dichloromethane; toluene; acetonitrile;