L-isoseryl-L-leucine benzyl ester hydrochloride

Base Information

Chemical Name:L-isoseryl-L-leucine benzyl ester hydrochloride
CAS No.:1365292-21-2
Molecular Formula:C₁₆H₂₄N₂O₄*ClH
Molecular Weight:344.838
Hs Code.:

Synonyms:L-isoseryl-L-leucine benzyl ester hydrochloride

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Chemical Property of L-isoseryl-L-leucine benzyl ester hydrochloride

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Technology Process of L-isoseryl-L-leucine benzyl ester hydrochloride

There total 3 articles about L-isoseryl-L-leucine benzyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.6%

: C₂₁H₃₂N₂O₆

: 1365292-21-2
L-isoseryl-L-leucine benzyl ester hydrochloride

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 0 - 20 ℃; for 7h;
DOI:10.3109/14756361003698147

Reference yield:

: 13139-15-6,53296-34-7
N-tert-butoxycarbonyl-L-leucine

: 1365292-21-2
L-isoseryl-L-leucine benzyl ester hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: tetra-(n-butyl)ammonium iodide; potassium carbonate; potassium iodide / acetone

2: hydrogenchloride / ethyl acetate

3: dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 13 h / 0 - 20 °C

4: hydrogenchloride / ethyl acetate / 7 h / 0 - 20 °C

With hydrogenchloride; dmap; tetra-(n-butyl)ammonium iodide; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium iodide; In dichloromethane; ethyl acetate; acetone;
DOI:10.3109/14756361003698147

Reference yield:

: 87746-56-3
2-tert-butoxycarbonylamino-4-methyl-penatnoic acid benzyl ester

: 1365292-21-2
L-isoseryl-L-leucine benzyl ester hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / ethyl acetate

2: dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 13 h / 0 - 20 °C

3: hydrogenchloride / ethyl acetate / 7 h / 0 - 20 °C

With hydrogenchloride; dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; ethyl acetate;
DOI:10.3109/14756361003698147