(S)-tert-butyl 1-(5-oxo-4,5-dihydrothiazol-2-yl)-2-phenylethylcarbamate

Base Information

Chemical Name:(S)-tert-butyl 1-(5-oxo-4,5-dihydrothiazol-2-yl)-2-phenylethylcarbamate
CAS No.:1355078-28-2
Molecular Formula:C₁₆H₂₀N₂O₃S
Molecular Weight:320.412
Hs Code.:

Synonyms:(S)-tert-butyl 1-(5-oxo-4,5-dihydrothiazol-2-yl)-2-phenylethylcarbamate

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Chemical Property of (S)-tert-butyl 1-(5-oxo-4,5-dihydrothiazol-2-yl)-2-phenylethylcarbamate

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Technology Process of (S)-tert-butyl 1-(5-oxo-4,5-dihydrothiazol-2-yl)-2-phenylethylcarbamate

There total 2 articles about (S)-tert-butyl 1-(5-oxo-4,5-dihydrothiazol-2-yl)-2-phenylethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: (S)-2-[2-(tert-butoxycarbonylamino)-3-phenylpropanethioamido]acetic acid

: 1355078-28-2
(S)-tert-butyl 1-(5-oxo-4,5-dihydrothiazol-2-yl)-2-phenylethylcarbamate

Guidance literature:: With dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1055/s-0031-1289594

Reference yield:

: 7625-57-2
methyl 2-((2S)-2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)acetate

: 1355078-28-2
(S)-tert-butyl 1-(5-oxo-4,5-dihydrothiazol-2-yl)-2-phenylethylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetraphosphorus decasulfide; sodium carbonate / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

2.1: sodium hydroxide / methanol; water / 16 h / 0 - 20 °C / Inert atmosphere

2.2: pH 1 / Inert atmosphere

3.1: dicyclohexyl-carbodiimide / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

With tetraphosphorus decasulfide; sodium carbonate; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; methanol; water;
DOI:10.1055/s-0031-1289594