C₃₇H₅₄N₄O₈Si

Base Information

Chemical Name:C₃₇H₅₄N₄O₈Si
CAS No.:1353660-71-5
Molecular Formula:C₃₇H₅₄N₄O₈Si
Molecular Weight:710.943
Hs Code.:

C<sub>37</sub>H<sub>54</sub>N<sub>4</sub>O<sub>8</sub>Si

Synonyms:C₃₇H₅₄N₄O₈Si

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Chemical Property of C₃₇H₅₄N₄O₈Si

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Technology Process of C₃₇H₅₄N₄O₈Si

There total 7 articles about C₃₇H₅₄N₄O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1353660-67-9
C₃₈H₅₆N₄O₈Si

: 1353660-71-5
C₃₇H₅₄N₄O₈Si

Guidance literature:: C₃₈H₅₆N₄O₈Si; With water; sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 2h; Inert atmosphere;

With sodium hydrogen sulfate; In tetrahydrofuran; methanol; water; ethyl acetate; pH=Ca. 2;
DOI:10.1002/chem.201101978

Reference yield:

: 1353660-31-7
(E)-methyl 4-[tert-butyldimethylsilyloxymethyl]cinnamate

: 1353660-71-5
C₃₇H₅₄N₄O₈Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydroquinidine 1 4-phthalazinediyl diether; potassium dioxotetrahydroxoosmate(VI); methanesulfonamide; water; potassium carbonate; potassium hydrogencarbonate; potassium hexacyanoferrate(III) / tert-butyl alcohol / 0 - 20 °C / Inert atmosphere

2.1: hydrogen azide; triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 23 h / -25 - 20 °C / Inert atmosphere

3.1: proton sponge / 1,2-dichloro-ethane / 40 °C / Inert atmosphere

4.1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C

5.1: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / -10 - 20 °C / Inert atmosphere

6.1: water; sodium hydroxide / tetrahydrofuran; methanol / 2 h / 20 °C / Inert atmosphere

6.2: pH Ca_. 2

With hydroquinidine 1 4-phthalazinediyl diether; hydrogen azide; potassium dioxotetrahydroxoosmate(VI); methanesulfonamide; palladium 10% on activated carbon; water; hydrogen; potassium carbonate; benzotriazol-1-ol; potassium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; sodium hydroxide; potassium hexacyanoferrate(III); diethylazodicarboxylate; In tetrahydrofuran; methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; 1.1: Sharpless dihydroxylation / 2.1: Mitsunobu reaction;
DOI:10.1002/chem.201101978

Reference yield:

: 1353660-32-8
(2S,3R)-methyl 3-(4-((tert-butyldimethylsilyloxy)methyl)phenyl)-2,3-dihydroxypropanoate

: 1353660-71-5
C₃₇H₅₄N₄O₈Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen azide; triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 23 h / -25 - 20 °C / Inert atmosphere

2.1: proton sponge / 1,2-dichloro-ethane / 40 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C

4.1: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / -10 - 20 °C / Inert atmosphere

5.1: water; sodium hydroxide / tetrahydrofuran; methanol / 2 h / 20 °C / Inert atmosphere

5.2: pH Ca_. 2

With hydrogen azide; palladium 10% on activated carbon; water; hydrogen; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; sodium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; 1.1: Mitsunobu reaction;
DOI:10.1002/chem.201101978