Technology Process of C24H36N2O*ClH
There total 8 articles about C24H36N2O*ClH which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: hydrazine / ethanol; water / Reflux; Inert atmosphere
2: chloroform / 0.5 h / 25 °C
3: methanol; sodium tetrahydroborate / 0 - 25 °C
4: hydrogenchloride / chloroform; water / 70 °C
5: chloroform / 0.5 h / 25 °C
6: methanol; sodium tetrahydroborate / 3 h / 0 - 40 °C
With
hydrogenchloride; methanol; sodium tetrahydroborate; hydrazine;
In
ethanol; chloroform; water;
DOI:10.1021/ol2005159
- Guidance literature:
-
Multi-step reaction with 4 steps
1: methanol; sodium tetrahydroborate / 0 - 25 °C
2: hydrogenchloride / chloroform; water / 70 °C
3: chloroform / 0.5 h / 25 °C
4: methanol; sodium tetrahydroborate / 3 h / 0 - 40 °C
With
hydrogenchloride; methanol; sodium tetrahydroborate;
In
chloroform; water;
DOI:10.1021/ol2005159
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride / chloroform; water / 70 °C
2: chloroform / 0.5 h / 25 °C
3: methanol; sodium tetrahydroborate / 3 h / 0 - 40 °C
With
hydrogenchloride; methanol; sodium tetrahydroborate;
In
chloroform; water;
DOI:10.1021/ol2005159