2,3-diphenyl-5-(3,4,5-tris(2-(2-ethoxyethoxy)ethoxy)-1-benzyloxypropyl)-1,4-bis(chloromethyl)benzene

Base Information

Chemical Name:2,3-diphenyl-5-(3,4,5-tris(2-(2-ethoxyethoxy)ethoxy)-1-benzyloxypropyl)-1,4-bis(chloromethyl)benzene
CAS No.:1376711-93-1
Molecular Formula:C₄₈H₆₄Cl₂O₁₀
Molecular Weight:871.936
Hs Code.:

Synonyms:2,3-diphenyl-5-(3,4,5-tris(2-(2-ethoxyethoxy)ethoxy)-1-benzyloxypropyl)-1,4-bis(chloromethyl)benzene

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Chemical Property of 2,3-diphenyl-5-(3,4,5-tris(2-(2-ethoxyethoxy)ethoxy)-1-benzyloxypropyl)-1,4-bis(chloromethyl)benzene

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Technology Process of 2,3-diphenyl-5-(3,4,5-tris(2-(2-ethoxyethoxy)ethoxy)-1-benzyloxypropyl)-1,4-bis(chloromethyl)benzene

There total 8 articles about 2,3-diphenyl-5-(3,4,5-tris(2-(2-ethoxyethoxy)ethoxy)-1-benzyloxypropyl)-1,4-bis(chloromethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1376712-03-6
2,3-diphenyl-5-(3,4,5-tris(2-(2-ethoxyethoxy)ethoxy)-1-benzyloxypropyl)-1,4-bis(hydroxymethyl)benzene

: 1376711-93-1
2,3-diphenyl-5-(3,4,5-tris(2-(2-ethoxyethoxy)ethoxy)-1-benzyloxypropyl)-1,4-bis(chloromethyl)benzene

Guidance literature:: With thionyl chloride; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/ma300640n

Reference yield:

: 1376712-00-3
C₂₅H₄₃ClO₉

: 1376711-93-1
2,3-diphenyl-5-(3,4,5-tris(2-(2-ethoxyethoxy)ethoxy)-1-benzyloxypropyl)-1,4-bis(chloromethyl)benzene

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutylammomium bromide; sodium hydride / tetrahydrofuran / 12 h / Inert atmosphere; Reflux

2: toluene / 12 h / Reflux; Inert atmosphere

3: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 °C / Inert atmosphere; Reflux

4: thionyl chloride / dichloromethane / 2 h / 20 °C

With lithium aluminium tetrahydride; thionyl chloride; tetrabutylammomium bromide; sodium hydride; In tetrahydrofuran; dichloromethane; toluene; 2: Diels-Alder reaction;
DOI:10.1021/ma300640n

Reference yield:

: 1376712-01-4
3,4,5-tris(2-(2-ethoxyethoxy)ethoxy)-1-benzyloxypent-4-yne

: 1376711-93-1
2,3-diphenyl-5-(3,4,5-tris(2-(2-ethoxyethoxy)ethoxy)-1-benzyloxypropyl)-1,4-bis(chloromethyl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 12 h / Reflux; Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 °C / Inert atmosphere; Reflux

3: thionyl chloride / dichloromethane / 2 h / 20 °C

With lithium aluminium tetrahydride; thionyl chloride; In tetrahydrofuran; dichloromethane; toluene; 1: Diels-Alder reaction;
DOI:10.1021/ma300640n