rac-4-(5-fluoro-2-methoxyphenyl)-2-hydroxy-4-methyl-2-trifluoromethyl-pentanal

Base Information

Chemical Name:rac-4-(5-fluoro-2-methoxyphenyl)-2-hydroxy-4-methyl-2-trifluoromethyl-pentanal
CAS No.:611231-08-4
Molecular Formula:C₁₄H₁₆F₄O₃
Molecular Weight:308.273
Hs Code.:

Synonyms:rac-4-(5-fluoro-2-methoxyphenyl)-2-hydroxy-4-methyl-2-trifluoromethyl-pentanal

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Chemical Property of rac-4-(5-fluoro-2-methoxyphenyl)-2-hydroxy-4-methyl-2-trifluoromethyl-pentanal

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Technology Process of rac-4-(5-fluoro-2-methoxyphenyl)-2-hydroxy-4-methyl-2-trifluoromethyl-pentanal

There total 2 articles about rac-4-(5-fluoro-2-methoxyphenyl)-2-hydroxy-4-methyl-2-trifluoromethyl-pentanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 271587-45-2
2-hydroxy-4-(5-fluoro-2-methoxyphenyl)-4-methyl-2-trifluoromethyl-pentanol

: 611231-08-4
rac-4-(5-fluoro-2-methoxyphenyl)-2-hydroxy-4-methyl-2-trifluoromethyl-pentanal

Guidance literature:: 2-hydroxy-4-(5-fluoro-2-methoxyphenyl)-4-methyl-2-trifluoromethyl-pentanol; With SO₃/pyridine complex; dimethyl sulfoxide; triethylamine; In dichloromethane; at 15 - 20 ℃; for 0.666667h;

With ammonium chloride; In dichloromethane; water; at 20 ℃; for 0.25h;

Reference yield:

: 217195-92-1
4-(5-fluoro-2-methoxyphenyl)-2-hydroxy-4-methyl-2-(trifluoromethyl)pentanoic acid ethyl ester

: 611231-08-4
rac-4-(5-fluoro-2-methoxyphenyl)-2-hydroxy-4-methyl-2-trifluoromethyl-pentanal

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran

2: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide

With lithium aluminium tetrahydride; sulfur trioxide pyridine complex; triethylamine; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide;