2-benzoylamino-2-benzoyloxymethyl-2-deoxy-3-O-benzoyl-5-O-(p-tolylsulphonyl)-D-lyxono-1,4-lactone

Base Information

Chemical Name:2-benzoylamino-2-benzoyloxymethyl-2-deoxy-3-O-benzoyl-5-O-(p-tolylsulphonyl)-D-lyxono-1,4-lactone
CAS No.:88278-44-8
Molecular Formula:C₃₄H₂₉NO₁₀S
Molecular Weight:643.671
Hs Code.:

Synonyms:2-benzoylamino-2-benzoyloxymethyl-2-deoxy-3-O-benzoyl-5-O-(p-tolylsulphonyl)-D-lyxono-1,4-lactone

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Chemical Property of 2-benzoylamino-2-benzoyloxymethyl-2-deoxy-3-O-benzoyl-5-O-(p-tolylsulphonyl)-D-lyxono-1,4-lactone

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Technology Process of 2-benzoylamino-2-benzoyloxymethyl-2-deoxy-3-O-benzoyl-5-O-(p-tolylsulphonyl)-D-lyxono-1,4-lactone

There total 15 articles about 2-benzoylamino-2-benzoyloxymethyl-2-deoxy-3-O-benzoyl-5-O-(p-tolylsulphonyl)-D-lyxono-1,4-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 82726-99-6
2-benzoylamino-2-benzoyloxymethyl-2-deoxy-3-O-benzoyl-D-lyxono-1,4-lactone

: 98-59-9
p-toluenesulfonyl chloride

: 88278-44-8
2-benzoylamino-2-benzoyloxymethyl-2-deoxy-3-O-benzoyl-5-O-(p-tolylsulphonyl)-D-lyxono-1,4-lactone

Guidance literature:: With dmap; triethylamine; In dichloromethane; at -10 ℃; for 1h;

Reference yield:

: 82726-90-7
2-deoxy-2-hydroxymethyl-2-p-toluidino-D-mannono-1,4-lactone

: 88278-44-8
2-benzoylamino-2-benzoyloxymethyl-2-deoxy-3-O-benzoyl-5-O-(p-tolylsulphonyl)-D-lyxono-1,4-lactone

Guidance literature:: Multi-step reaction with 8 steps

1: 80 percent / H₂, 1 M HCl / Pd-C

2: 2.) Et₃N / 1.) pyridine, 2.) CH₃OH

3: 90 percent / H₂SO₄

4: 90 percent / pyridine

5: 90 percent / acetic acid / tetrahydrofuran; H₂O

6: 100 percent / Na periodate

7: 100 percent / NaBH₃CN / tetrahydrofuran

8: 95 percent / 4-(dimethylamino)-pyridine, Et₃N / CH₂Cl₂ / -20 °C

With hydrogenchloride; dmap; sodium periodate; sulfuric acid; hydrogen; sodium cyanoborohydride; acetic acid; triethylamine; palladium on activated charcoal; In tetrahydrofuran; pyridine; dichloromethane; water;
DOI:10.1039/c39820000488

Reference yield:

: 57-48-7,18875-34-8
D-Fructose

: 88278-44-8
2-benzoylamino-2-benzoyloxymethyl-2-deoxy-3-O-benzoyl-5-O-(p-tolylsulphonyl)-D-lyxono-1,4-lactone

Guidance literature:: Multi-step reaction with 10 steps

2: 90 percent / conc. HCl / 40 h

3: 80 percent / H₂, 1 M HCl / Pd-C

4: 2.) Et₃N / 1.) pyridine, 2.) CH₃OH

5: 90 percent / H₂SO₄

6: 90 percent / pyridine

7: 90 percent / acetic acid / tetrahydrofuran; H₂O

8: 100 percent / Na periodate

9: 100 percent / NaBH₃CN / tetrahydrofuran

10: 95 percent / 4-(dimethylamino)-pyridine, Et₃N / CH₂Cl₂ / -20 °C

With hydrogenchloride; dmap; sodium periodate; sulfuric acid; hydrogen; sodium cyanoborohydride; acetic acid; triethylamine; palladium on activated charcoal; In tetrahydrofuran; pyridine; dichloromethane; water;
DOI:10.1039/c39820000488