Phosphine, 1,8-anthracenediylbis[diphenyl-

Base Information

Chemical Name:Phosphine, 1,8-anthracenediylbis[diphenyl-
CAS No.:131276-25-0
Molecular Formula:C₃₈H₂₈P₂
Molecular Weight:546.588
Hs Code.:
DSSTox Substance ID:DTXSID901222143
Nikkaji Number:J944.161A

Synonyms:Phosphine, 1,8-anthracenediylbis[diphenyl-;SCHEMBL3676836;DTXSID901222143;1,8-bis(diphenylphosphino)anthracene;1,8-bis(diphenyl-phosphino)anthracene;[8-(Diphenylphosphino)-1-anthryl](diphenyl)phosphine #;1,1'-(1,8-Anthracenediyl)bis[1,1-diphenylphosphine];131276-25-0

Suppliers and Price of Phosphine, 1,8-anthracenediylbis[diphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phosphine, 1,8-anthracenediylbis[diphenyl-

Chemical Property:

XLogP3:9.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:6
Exact Mass:546.16662489
Heavy Atom Count:40
Complexity:658

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)P(C2=CC=CC=C2)C3=CC=CC4=CC5=C(C=C43)C(=CC=C5)P(C6=CC=CC=C6)C7=CC=CC=C7

Technology Process of Phosphine, 1,8-anthracenediylbis[diphenyl-

There total 5 articles about Phosphine, 1,8-anthracenediylbis[diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 15475-27-1,4346-39-8
potassium diphenylphosphine

: 204506-83-2
1,8-difluoroanthracene

: 131276-25-0
1,8-bis-(diphenylphosphino)anthracene

Guidance literature:: In tetrahydrofuran; 1,4-dioxane; for 3h; Heating;
DOI:10.1055/s-1998-1627

Reference yield: 64.0%

: 131276-24-9
1,8-dibromoanthraquinone

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 131276-25-0
1,8-bis-(diphenylphosphino)anthracene

Guidance literature:: 1,8-dibromoanthraquinone; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1.08333h;

chloro-diphenylphosphine; In tetrahydrofuran; at -78 ℃; Reflux;

Reference yield:

: 82-43-9
1,8-dichloroanthraquinone

: 131276-25-0
1,8-bis-(diphenylphosphino)anthracene

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / CsF / dimethylsulfoxide / 14 h / 137 °C

2: 84 percent / Zn, NH₃/H₂₀ / 4 h / 75 °C

3: 86 percent / dioxane; tetrahydrofuran / 3 h / Heating

With ammonia; water; cesium fluoride; zinc; In tetrahydrofuran; 1,4-dioxane; dimethyl sulfoxide;
DOI:10.1055/s-1998-1627