[(C₅(CH₃)5)(((CH₃)3C)3PNC₆H₄)TiCl]⁽¹⁺⁾*[B(C₆F₅)4]^(1-)=[(C₅(CH₃)5)(((CH₃)3C)3PNC₆H₄)TiCl][B(C₆F₅)4]

Base Information

• Chemical Name: [(C₅(CH₃)5)(((CH₃)3C)3PNC₆H₄)TiCl]⁽¹⁺⁾*[B(C₆F₅)4]^(1-)=[(C₅(CH₃)5)(((CH₃)3C)3PNC₆H₄)TiCl][B(C₆F₅)4]
• CAS No.: 882534-92-1
• Molecular Formula: C₂₄BF₂₀*C₂₈H₄₆ClNPTi
• Molecular Weight: 1190.03

Synonyms:[(C₅(CH₃)5)(((CH₃)3C)3PNC₆H₄)TiCl]⁽¹⁺⁾*[B(C₆F₅)4]^(1-)=[(C₅(CH₃)5)(((CH₃)3C)3PNC₆H₄)TiCl][B(C₆F₅)4]

Chemical Property of [(C₅(CH₃)5)(((CH₃)3C)3PNC₆H₄)TiCl]⁽¹⁺⁾*[B(C₆F₅)4]^(1-)=[(C₅(CH₃)5)(((CH₃)3C)3PNC₆H₄)TiCl][B(C₆F₅)4]

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Technology Process of [(C₅(CH₃)5)(((CH₃)3C)3PNC₆H₄)TiCl]⁽¹⁺⁾*[B(C₆F₅)4]^(1-)=[(C₅(CH₃)5)(((CH₃)3C)3PNC₆H₄)TiCl][B(C₆F₅)4]

There total 3 articles about [(C₅(CH₃)5)(((CH₃)3C)3PNC₆H₄)TiCl]⁽¹⁺⁾*[B(C₆F₅)4]^(1-)=[(C₅(CH₃)5)(((CH₃)3C)3PNC₆H₄)TiCl][B(C₆F₅)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

[Cp(*)((t)Bu3P=N)Ti(2-Cl-C6H4)][B(C6F5)4] (882534-84-1) → [Cp(*)((t)Bu3P=N)TiCl][B(C6F5)4] (882534-79-4) + [(C5(CH3)5)(((CH3)3C)3PNC6H4)TiCl](1+)*[B(C6F5)4](1-)=[(C5(CH3)5)(((CH3)3C)3PNC6H4)TiCl][B(C6F5)4] (882534-92-1)

Guidance literature:

In chlorobenzene; (Ar); stirred at room temp. for 3 d; hexanes added, crystd. at -30°C; elem. anal.;

DOI:10.1021/ja0583618

Reference yield:

[Cp(*)((t)Bu3P=N)Ti(2-Cl-C6H4)][B(C6F5)4] (882534-84-1) → [(C5(CH3)5)(((CH3)3C)3PNC6H4)TiCl](1+)*[B(C6F5)4](1-)=[(C5(CH3)5)(((CH3)3C)3PNC6H4)TiCl][B(C6F5)4] (882534-92-1)

Guidance literature:

In further solvent(s); (Ar); monitored by NMR in C6D5Br at 292-332 K; not isolated; Kinetics;

DOI:10.1021/ja0583618

Reference yield:

[Cp(*)((t)Bu3P=N)Ti(2-Cl-C6H4)(THF)][B(C6F5)4]*THF (882534-95-4) → [(C5(CH3)5)(((CH3)3C)3PNC6H4)TiCl](1+)*[B(C6F5)4](1-)=[(C5(CH3)5)(((CH3)3C)3PNC6H4)TiCl][B(C6F5)4] (882534-92-1) + [Cp(*)((t)Bu3P=N)TiCl(THF)][B(C6F5)4] (882534-81-8)

Guidance literature:

In not given;

DOI:10.1021/ja0583618

upstream raw materials:

[Cp(*)((t)Bu₃P=N)Ti(2-Cl-C₆H₄)][B(C₆F₅)4]

[Cp(*)((t)Bu₃P=N)Ti(2-Cl-C₆H₄)(THF)][B(C₆F₅)4]*THF

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