3-(4-cyclopropylphenylmethyl)-1-(β-D-glucopyranosyl)indole

Base Information

Chemical Name:3-(4-cyclopropylphenylmethyl)-1-(β-D-glucopyranosyl)indole
CAS No.:1452838-63-9
Molecular Formula:C₂₄H₂₇NO₅
Molecular Weight:409.482
Hs Code.:

Synonyms:3-(4-cyclopropylphenylmethyl)-1-(β-D-glucopyranosyl)indole

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Chemical Property of 3-(4-cyclopropylphenylmethyl)-1-(β-D-glucopyranosyl)indole

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Technology Process of 3-(4-cyclopropylphenylmethyl)-1-(β-D-glucopyranosyl)indole

There total 8 articles about 3-(4-cyclopropylphenylmethyl)-1-(β-D-glucopyranosyl)indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1493759-35-5
C₃₂H₃₅NO₉

: 1452838-63-9
3-(4-cyclopropylphenylmethyl)-1-(β-D-glucopyranosyl)indole

Guidance literature:: With methanol; sodium methylate; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1021/ml400339b

Reference yield:

: 496-15-1
1-indoline

: 1452838-63-9
3-(4-cyclopropylphenylmethyl)-1-(β-D-glucopyranosyl)indole

Guidance literature:: Multi-step reaction with 7 steps

1.1: ethanol; water / Reflux; Inert atmosphere

2.1: pyridine; dmap / chloroform / 20 °C

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / water; 1,4-dioxane / 20 °C

4.1: trichlorophosphate / 1,2-dichloro-ethane / 70 °C

5.1: magnesium; ethylene dibromide / tetrahydrofuran / 20 °C / Inert atmosphere

5.2: Inert atmosphere; Cooling with ice

6.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / Inert atmosphere; Cooling with ice

7.1: sodium methylate; methanol / tetrahydrofuran / 20 °C / Inert atmosphere

With pyridine; methanol; triethylsilane; dmap; boron trifluoride diethyl etherate; sodium methylate; magnesium; ethylene dibromide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; chloroform; water; 1,2-dichloro-ethane; acetonitrile; 4.1: |Vilsmeier-Haack Formylation;
DOI:10.1021/ml400339b

Reference yield:

: 22855-03-4,23477-48-7,38730-31-3,38740-49-7
1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)indoline

: 1452838-63-9
3-(4-cyclopropylphenylmethyl)-1-(β-D-glucopyranosyl)indole

Guidance literature:: Multi-step reaction with 5 steps

1.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / water; 1,4-dioxane / 20 °C

2.1: trichlorophosphate / 1,2-dichloro-ethane / 70 °C

3.1: magnesium; ethylene dibromide / tetrahydrofuran / 20 °C / Inert atmosphere

3.2: Inert atmosphere; Cooling with ice

4.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / Inert atmosphere; Cooling with ice

5.1: sodium methylate; methanol / tetrahydrofuran / 20 °C / Inert atmosphere

With methanol; triethylsilane; boron trifluoride diethyl etherate; sodium methylate; magnesium; ethylene dibromide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; 1,2-dichloro-ethane; acetonitrile; 2.1: |Vilsmeier-Haack Formylation;
DOI:10.1021/ml400339b