7,7,7-tris(3,5-di-tert-butylphenyl)hepta-1,3,5-triyne

Base Information

• Chemical Name: 7,7,7-tris(3,5-di-tert-butylphenyl)hepta-1,3,5-triyne
• CAS No.: 1257847-38-3
• Molecular Formula: C₄₉H₆₄
• Molecular Weight: 653.047
• Mol file: 1257847-38-3.mol

Synonyms:7,7,7-tris(3,5-di-tert-butylphenyl)hepta-1,3,5-triyne

Chemical Property of 7,7,7-tris(3,5-di-tert-butylphenyl)hepta-1,3,5-triyne

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 7,7,7-tris(3,5-di-tert-butylphenyl)hepta-1,3,5-triyne

There total 1 articles about 7,7,7-tris(3,5-di-tert-butylphenyl)hepta-1,3,5-triyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

C58H84Si (1257847-47-4) → 7,7,7-tris(3,5-di-tert-butylphenyl)hepta-1,3,5-triyne (1257847-38-3)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;

DOI:10.1038/nchem.828

Reference yield: 89.0%

7,7,7-tris(3,5-di-tert-butylphenyl)hepta-1,3,5-triyne (1257847-38-3) + [chloro][5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato]gallium(III) → [7,7,7-tris(3,5-di-tert-butylphenyl)hepta-1,3,5-triyn-1-ide][5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato]gallium(III)

Guidance literature:

7,7,7-tris(3,5-di-tert-butylphenyl)hepta-1,3,5-triyne; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 0.333333h;

[chloro][5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato]gallium(III); In tetrahydrofuran; hexane; toluene; at 20 ℃; for 0.166667h;

DOI:10.1002/anie.201812142

Reference yield: 73.0%

1-triisopropylsilanyl-8-trimethylsilanyl-octa-1,3,5,7-tetrayne + 7,7,7-tris(3,5-di-tert-butylphenyl)hepta-1,3,5-triyne (1257847-38-3) → C66H84Si (1257847-50-9)

Guidance literature:

With 2,6-dimethylpyridine; methanol; copper(II) acetate monohydrate; potassium carbonate; In dichloromethane; at 20 ℃; for 17h;

DOI:10.1038/nchem.828

upstream raw materials:

C₅₈H₈₄Si

Downstream raw materials:

C₆₆H₈₄Si

C₉₈H₁₂₆

C₆₄H₈₄Si