N-{4-[cyclopropyl(hydroxy)methyl]-2,6-dimethylphenyl}-N,N-dimethylimidoformamide

Base Information

Chemical Name:N-{4-[cyclopropyl(hydroxy)methyl]-2,6-dimethylphenyl}-N,N-dimethylimidoformamide
CAS No.:1139573-91-3
Molecular Formula:C₁₅H₂₂N₂O
Molecular Weight:246.352
Hs Code.:

Synonyms:N-{4-[cyclopropyl(hydroxy)methyl]-2,6-dimethylphenyl}-N,N-dimethylimidoformamide

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Chemical Property of N-{4-[cyclopropyl(hydroxy)methyl]-2,6-dimethylphenyl}-N,N-dimethylimidoformamide

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Technology Process of N-{4-[cyclopropyl(hydroxy)methyl]-2,6-dimethylphenyl}-N,N-dimethylimidoformamide

There total 1 articles about N-{4-[cyclopropyl(hydroxy)methyl]-2,6-dimethylphenyl}-N,N-dimethylimidoformamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 114886-15-6
N'-(4-bromo-2,6-dimethylphenyl)-N,N-dimethylmethanimidamide

: 1489-69-6
Cyclopropanecarboxaldehyde

: 1139573-91-3
N-{4-[cyclopropyl(hydroxy)methyl]-2,6-dimethylphenyl}-N,N-dimethylimidoformamide

Guidance literature:: N'-(4-bromo-2,6-dimethylphenyl)-N,N-dimethylmethanimidamide; With n-butyllithium; In tetrahydrofuran; hexanes; at -70 - -50 ℃; for 0.666667h;

Cyclopropanecarboxaldehyde; In tetrahydrofuran; hexanes; at -70 - 20 ℃; for 0.5h;

With water; In tetrahydrofuran; hexanes; at 0 - 20 ℃; Product distribution / selectivity;

Reference yield:

: 1139573-91-3
N-{4-[cyclopropyl(hydroxy)methyl]-2,6-dimethylphenyl}-N,N-dimethylimidoformamide

: 1139573-86-6
(4-amino-3,5-dimethylphenyl)(cyclopropyl)methanol

Guidance literature:: N-{4-[cyclopropyl(hydroxy)methyl]-2,6-dimethylphenyl}-N,N-dimethylimidoformamide; With lithium hydroxide; ethanolamine; In tetrahydrofuran; hexanes; water; isopropyl alcohol; for 18h; Heating / reflux;

With hydrogenchloride; In tetrahydrofuran; hexanes; water; isopropyl alcohol; at 20 ℃; pH=~ 10; Product distribution / selectivity;