Technology Process of C30H37BrF2N4O6
There total 5 articles about C30H37BrF2N4O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C11H10BrNO4;
With
benzotriazol-1-ol; dicyclohexyl-carbodiimide;
In
dichloromethane;
at 0 ℃;
for 1h;
Inert atmosphere;
C19H29F2N3O3;
In
dichloromethane;
at 0 - 20 ℃;
Inert atmosphere;
- Guidance literature:
-
C13H14BrNO4;
With
benzotriazol-1-ol; dicyclohexyl-carbodiimide;
In
dichloromethane;
at 0 ℃;
for 1h;
Inert atmosphere;
C19H29F2N3O3;
In
dichloromethane;
at 20 ℃;
for 6.25h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydroxide; water / 1,4-dioxane / 5 h / 20 °C / Reflux
2.1: trifluoroacetic anhydride / 4.5 h / 0 - 20 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere
3.1: triethylamine; diphenyl phosphoryl azide / benzene / 4 h / 20 °C / Inert atmosphere; Reflux
4.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 1 h / 0 °C / Inert atmosphere
4.2: 6.25 h / 20 °C
With
diphenyl phosphoryl azide; water; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic anhydride; sodium hydroxide;
In
1,4-dioxane; dichloromethane; benzene;