5-[(2,4-diisobutoxy-5-nitro-benzoyl)-(2,4-dimethoxybenzyl)-amino]-2,4-dimethoxybenzoic acid

Base Information

Chemical Name:5-[(2,4-diisobutoxy-5-nitro-benzoyl)-(2,4-dimethoxybenzyl)-amino]-2,4-dimethoxybenzoic acid
CAS No.:915184-70-2
Molecular Formula:C₃₃H₄₀N₂O₁₁
Molecular Weight:640.687
Hs Code.:

Synonyms:5-[(2,4-diisobutoxy-5-nitro-benzoyl)-(2,4-dimethoxybenzyl)-amino]-2,4-dimethoxybenzoic acid

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Chemical Property of 5-[(2,4-diisobutoxy-5-nitro-benzoyl)-(2,4-dimethoxybenzyl)-amino]-2,4-dimethoxybenzoic acid

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Technology Process of 5-[(2,4-diisobutoxy-5-nitro-benzoyl)-(2,4-dimethoxybenzyl)-amino]-2,4-dimethoxybenzoic acid

There total 6 articles about 5-[(2,4-diisobutoxy-5-nitro-benzoyl)-(2,4-dimethoxybenzyl)-amino]-2,4-dimethoxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 915184-67-7
5-[(2,4-diisobutoxy-5-nitro-benzoyl)-(2,4-dimethoxy-benzyl)-amino]-2,4-dimethoxy-benzoic acid methyl ester

: 915184-70-2
5-[(2,4-diisobutoxy-5-nitro-benzoyl)-(2,4-dimethoxybenzyl)-amino]-2,4-dimethoxybenzoic acid

Guidance literature:: With sodium hydroxide; In methanol; at 20 ℃;
DOI:10.1021/ol062103d

Reference yield:

: 81574-75-6
2,4-dimethoxy-5-nitro-benzoic acid methyl ester

: 915184-70-2
5-[(2,4-diisobutoxy-5-nitro-benzoyl)-(2,4-dimethoxybenzyl)-amino]-2,4-dimethoxybenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: H₂ / Pd/C

2.1: ethanol

2.2: 95 percent / NaBH₄ / ethanol

3.1: 95 percent / Et₃N / CH₂Cl₂

4.1: aq. NaOH / methanol / 20 °C

With sodium hydroxide; hydrogen; triethylamine; palladium on activated charcoal; In methanol; ethanol; dichloromethane;
DOI:10.1021/ol062103d

Reference yield:

: 874210-18-1
2,4-diisobutoxy-5-nitrobenzoic acid

: 915184-70-2
5-[(2,4-diisobutoxy-5-nitro-benzoyl)-(2,4-dimethoxybenzyl)-amino]-2,4-dimethoxybenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: (COCl)2; DMF / CH₂Cl₂ / Heating

2: 95 percent / Et₃N / CH₂Cl₂

3: aq. NaOH / methanol / 20 °C

With sodium hydroxide; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In methanol; dichloromethane;
DOI:10.1021/ol062103d