2,9,16,23-tetrakis(N-benzyl-4-phenyloxyacetamide)phthalocyaninatocobalt(II)

Base Information

Chemical Name:2,9,16,23-tetrakis(N-benzyl-4-phenyloxyacetamide)phthalocyaninatocobalt(II)
CAS No.:947733-59-7
Molecular Formula:C₉₂H₆₈CoN₁₂O₈
Molecular Weight:1528.62
Hs Code.:

Synonyms:2,9,16,23-tetrakis(N-benzyl-4-phenyloxyacetamide)phthalocyaninatocobalt(II)

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Chemical Property of 2,9,16,23-tetrakis(N-benzyl-4-phenyloxyacetamide)phthalocyaninatocobalt(II)

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Technology Process of 2,9,16,23-tetrakis(N-benzyl-4-phenyloxyacetamide)phthalocyaninatocobalt(II)

There total 1 articles about 2,9,16,23-tetrakis(N-benzyl-4-phenyloxyacetamide)phthalocyaninatocobalt(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.3%

: 947733-55-3
2,9,16,23-tetrakis(4-phenyloxyacetic acid)phthalocyaninatocobalt(II)

: 100-46-9
benzylamine

: 947733-59-7
2,9,16,23-tetrakis(N-benzyl-4-phenyloxyacetamide)phthalocyaninatocobalt(II)

Guidance literature:: With thionyl chloride; In tetrahydrofuran; metal-compd. was refluxed in SOCl2 for 4 h, excess of SOCl2 was removed in vac., solid was dissolved in dry THF, benzylamine in dry THF was dropped at 10 °C, stirring at room temp. for 15-16 h; THF was removed in vac., H2O was added, ppt. was filtered off, washed with H2O, MeOH, MeCN and Et2O, dried, elem. anal.;
DOI:10.1016/j.poly.2007.01.010