7-(4-{3-[2-(3-bromo-phenyl)-2-hydroxyethyl]-3H-[1,2,3]triazol-4-yl}phenylcarbamoyl)heptanoic acid methyl ester

Base Information

• Chemical Name: 7-(4-{3-[2-(3-bromo-phenyl)-2-hydroxyethyl]-3H-[1,2,3]triazol-4-yl}phenylcarbamoyl)heptanoic acid methyl ester
• CAS No.: 1033391-49-9
• Molecular Formula: C₂₅H₂₉BrN₄O₄
• Molecular Weight: 529.434

Synonyms:7-(4-{3-[2-(3-bromo-phenyl)-2-hydroxyethyl]-3H-[1,2,3]triazol-4-yl}phenylcarbamoyl)heptanoic acid methyl ester

Chemical Property of 7-(4-{3-[2-(3-bromo-phenyl)-2-hydroxyethyl]-3H-[1,2,3]triazol-4-yl}phenylcarbamoyl)heptanoic acid methyl ester

Chemical Property:

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Technology Process of 7-(4-{3-[2-(3-bromo-phenyl)-2-hydroxyethyl]-3H-[1,2,3]triazol-4-yl}phenylcarbamoyl)heptanoic acid methyl ester

There total 1 articles about 7-(4-{3-[2-(3-bromo-phenyl)-2-hydroxyethyl]-3H-[1,2,3]triazol-4-yl}phenylcarbamoyl)heptanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

2-azido-1-(3-bromophenyl)ethanol (943911-72-6) + 7-(4-ethynylphenylcarbamoyl)heptanoic acid methyl ester (1033390-80-5) → 7-(4-{3-[2-(3-bromo-phenyl)-2-hydroxyethyl]-3H-[1,2,3]triazol-4-yl}phenylcarbamoyl)heptanoic acid methyl ester (1033391-49-9)

Guidance literature:

With chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II); In tetrahydrofuran; for 8h; Reflux; Inert atmosphere;

DOI:10.1021/jm701606b

Reference yield: 41.0%

7-(4-{3-[2-(3-bromo-phenyl)-2-hydroxyethyl]-3H-[1,2,3]triazol-4-yl}phenylcarbamoyl)heptanoic acid methyl ester (1033391-49-9) → octanedioic acid (4-{3-[2-(3-bromophenyl)-2-hydroxyethyl]-3H-[1,2,3]triazol-4-yl}phenyl)amide hydroxyamide (1033391-04-6)

Guidance literature:

With potassium hydroxide; hydroxylamine hydrochloride; In methanol; at 20 ℃; for 0.5h;

DOI:10.1021/jm701606b

upstream raw materials:

2-azido-1-(3-bromophenyl)ethanol

7-(4-ethynylphenylcarbamoyl)heptanoic acid methyl ester

Downstream raw materials:

octanedioic acid (4-{3-[2-(3-bromophenyl)-2-hydroxyethyl]-3H-[1,2,3]triazol-4-yl}phenyl)amide hydroxyamide

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