tetrakis[4-(N-tert-butyl-N-oxyamino)phenyl]methane tetraradical

Base Information

Chemical Name:tetrakis[4-(N-tert-butyl-N-oxyamino)phenyl]methane tetraradical
CAS No.:358618-99-2
Molecular Formula:C₄₁H₅₂N₄O₄
Molecular Weight:664.888
Hs Code.:

Synonyms:tetrakis[4-(N-tert-butyl-N-oxyamino)phenyl]methane tetraradical

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Chemical Property of tetrakis[4-(N-tert-butyl-N-oxyamino)phenyl]methane tetraradical

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Technology Process of tetrakis[4-(N-tert-butyl-N-oxyamino)phenyl]methane tetraradical

There total 2 articles about tetrakis[4-(N-tert-butyl-N-oxyamino)phenyl]methane tetraradical which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tetrakis[4-(N-tert-butyl-N-hydroxyamino)phenyl]methane

: 358618-99-2
tetrakis[4-(N-tert-butyl-N-oxyamino)phenyl]methane tetraradical

Guidance literature:: With sodium periodate; In dichloromethane; for 0.5h;
DOI:10.1021/ja016133h

Reference yield:

: 105309-59-9
tetrakis(4-bromophenyl)methane

: 358618-99-2
tetrakis[4-(N-tert-butyl-N-oxyamino)phenyl]methane tetraradical

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / 20 °C

1.2: hexane; tetrahydrofuran / 12 h / 20 °C

2.1: aq. NaIO₄ / CH₂Cl₂ / 0.5 h

With sodium periodate; n-butyllithium; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ja016133h

Reference yield:

: manganese(II) hexafluoroacetylacetonate dihydrate

: 358618-99-2
tetrakis[4-(N-tert-butyl-N-oxyamino)phenyl]methane tetraradical

: (C₄H₉NOC₆H₄)4C(Mn(CF₃COCHCOCF₃)2)2

Guidance literature:: In n-heptane; dichloromethane; a soln. of Mn-complex in heptane was boiled to removed hydratation H2O, few drops of CH2Cl2 were added, cooled to room temp., added to a soln. of tetranitroxide in CH2Cl2, 10 d; elem. anal.;
DOI:10.1021/ja016133h