2-Imino-3-(4-methoxy-benzyl)-1-methyl-2,3-dihydro-1H-indol-3-yl-hydroperoxide

Base Information

Chemical Name:2-Imino-3-(4-methoxy-benzyl)-1-methyl-2,3-dihydro-1H-indol-3-yl-hydroperoxide
CAS No.:76689-83-3
Molecular Formula:C₁₇H₁₈N₂O₃
Molecular Weight:298.342
Hs Code.:

Synonyms:2-Imino-3-(4-methoxy-benzyl)-1-methyl-2,3-dihydro-1H-indol-3-yl-hydroperoxide

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Chemical Property of 2-Imino-3-(4-methoxy-benzyl)-1-methyl-2,3-dihydro-1H-indol-3-yl-hydroperoxide

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Technology Process of 2-Imino-3-(4-methoxy-benzyl)-1-methyl-2,3-dihydro-1H-indol-3-yl-hydroperoxide

There total 3 articles about 2-Imino-3-(4-methoxy-benzyl)-1-methyl-2,3-dihydro-1H-indol-3-yl-hydroperoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 76689-80-0
3-(4-methoxybenzyl)-1-methylindolin-2-imine hydrochloride

: 76689-83-3
2-Imino-3-(4-methoxy-benzyl)-1-methyl-2,3-dihydro-1H-indol-3-yl-hydroperoxide

Guidance literature:: With sodium hydroxide; oxygen; In water; for 6h;
DOI:10.1007/BF00742837

Reference yield:

: 15893-42-2
3-(4-methoxyphenyl)propionyl chloride

: 76689-83-3
2-Imino-3-(4-methoxy-benzyl)-1-methyl-2,3-dihydro-1H-indol-3-yl-hydroperoxide

Guidance literature:: Multi-step reaction with 3 steps

1: 47 percent / Et₃N / benzene / Heating

2: 60 percent / POCl₃ / dioxane / 2 h / Heating

3: 71 percent / O₂/NaOH / H₂O / 6 h

With sodium hydroxide; oxygen; triethylamine; trichlorophosphate; In 1,4-dioxane; water; benzene;
DOI:10.1007/BF00742837

Reference yield:

: 76689-76-4
3-(4-Methoxy-phenyl)-propionic acid N'-methyl-N'-phenyl-hydrazide

: 76689-83-3
2-Imino-3-(4-methoxy-benzyl)-1-methyl-2,3-dihydro-1H-indol-3-yl-hydroperoxide

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / POCl₃ / dioxane / 2 h / Heating

2: 71 percent / O₂/NaOH / H₂O / 6 h

With sodium hydroxide; oxygen; trichlorophosphate; In 1,4-dioxane; water;
DOI:10.1007/BF00742837