Technology Process of C80H103BF2IN5
There total 8 articles about C80H103BF2IN5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
piperidine; toluene-4-sulfonic acid;
In
toluene;
at 140 ℃;
Inert atmosphere;
DOI:10.1021/ol202443g
- Guidance literature:
-
Multi-step reaction with 5 steps
1: N-Bromosuccinimide / chloroform / Inert atmosphere
2: trichlorophosphate / Reflux; Inert atmosphere
3: palladium on activated charcoal; sodium formate / tetrahydrofuran / Reflux; Inert atmosphere
4: bis-triphenylphosphine-palladium(II) chloride; sodium formate / N,N-dimethyl-formamide / Inert atmosphere; Heating
5: piperidine; toluene-4-sulfonic acid / toluene / 140 °C / Inert atmosphere
With
piperidine; bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; palladium on activated charcoal; sodium formate; toluene-4-sulfonic acid; trichlorophosphate;
In
tetrahydrofuran; chloroform; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol202443g
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium carbonate / N,N-dimethyl-formamide / Inert atmosphere
2: N-Bromosuccinimide / chloroform / Inert atmosphere
3: trichlorophosphate / Reflux; Inert atmosphere
4: palladium on activated charcoal; sodium formate / tetrahydrofuran / Reflux; Inert atmosphere
5: bis-triphenylphosphine-palladium(II) chloride; sodium formate / N,N-dimethyl-formamide / Inert atmosphere; Heating
6: piperidine; toluene-4-sulfonic acid / toluene / 140 °C / Inert atmosphere
With
piperidine; bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; palladium on activated charcoal; sodium formate; potassium carbonate; toluene-4-sulfonic acid; trichlorophosphate;
In
tetrahydrofuran; chloroform; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol202443g