{3-[4-(2-Benzyloxycarbonylamino-acetylamino)-butylamino]-propyl}-carbamic acid tert-butyl ester

Base Information

• Chemical Name: {3-[4-(2-Benzyloxycarbonylamino-acetylamino)-butylamino]-propyl}-carbamic acid tert-butyl ester
• CAS No.: 1071125-15-9
• Molecular Formula: C₂₂H₃₆N₄O₅
• Molecular Weight: 436.552

Synonyms:{3-[4-(2-Benzyloxycarbonylamino-acetylamino)-butylamino]-propyl}-carbamic acid tert-butyl ester

Chemical Property of {3-[4-(2-Benzyloxycarbonylamino-acetylamino)-butylamino]-propyl}-carbamic acid tert-butyl ester

Chemical Property:

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Technology Process of {3-[4-(2-Benzyloxycarbonylamino-acetylamino)-butylamino]-propyl}-carbamic acid tert-butyl ester

There total 3 articles about {3-[4-(2-Benzyloxycarbonylamino-acetylamino)-butylamino]-propyl}-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(benzyloxycarbonyl)glycyl-N4-(tert-butoxycarbonyl)putrescine (53412-33-2) → {3-[4-(2-Benzyloxycarbonylamino-acetylamino)-butylamino]-propyl}-carbamic acid tert-butyl ester (1071125-15-9)

Guidance literature:

Multi-step reaction with 2 steps

1: CF₃COOH / CH₂Cl₂ / 0.33 h / Ambient temperature

2: Et₃N, sodium cyanoborohydride / methanol / 13 h / Ambient temperature

With sodium cyanoborohydride; triethylamine; trifluoroacetic acid; In methanol; dichloromethane;

DOI:10.1021/ja00029a031

Reference yield:

N-(tert-butoxycarbonyl)-3-aminopropanal (58885-60-2) + [(4-Amino-butylcarbamoyl)-methyl]-carbamic acid benzyl ester; compound with trifluoro-acetic acid → {3-[4-(2-Benzyloxycarbonylamino-acetylamino)-butylamino]-propyl}-carbamic acid tert-butyl ester (1071125-15-9)

Guidance literature:

With sodium cyanoborohydride; triethylamine; In methanol; for 13h; Ambient temperature;

DOI:10.1021/ja00029a031

Reference yield:

N-(tert-butoxycarbonyl)-3-aminopropanal (58885-60-2) + [(4-Amino-butylcarbamoyl)-methyl]-carbamic acid benzyl ester → {3-[4-(2-Benzyloxycarbonylamino-acetylamino)-butylamino]-propyl}-carbamic acid tert-butyl ester (1071125-15-9)

Guidance literature:

With sodium cyanoborohydride; In methanol;

DOI:10.1016/S0040-4039(00)94727-0

upstream raw materials:

N-(tert-butoxycarbonyl)-3-aminopropanal

N-(benzyloxycarbonyl)glycyl-N⁴-(tert-butoxycarbonyl)putrescine

Downstream raw materials:

10-<(1,1-dimethylethoxy)carbonyl>-4-oxo-2,5,10,14-tetraazapentadecanedioic acid, 1-phenylmethyl 15-(1,1-dimethylethyl) ester

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