Technology Process of C27H38N2O5
There total 3 articles about C27H38N2O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 0 - 25 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/ja1071916
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydroxylamine monohydrate; ethylamine; copper(l) chloride / tetrahydrofuran; methanol / 3 h / 0 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 - 25 °C / Inert atmosphere
With
hydroxylamine monohydrate; tetrabutyl ammonium fluoride; ethylamine; copper(l) chloride;
In
tetrahydrofuran; methanol;
DOI:10.1021/ja1071916
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere
1.2: 2 h / -78 °C / Inert atmosphere
2.1: hydroxylamine monohydrate; ethylamine; copper(l) chloride / tetrahydrofuran; methanol / 3 h / 0 °C / Inert atmosphere
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 - 25 °C / Inert atmosphere
With
n-butyllithium; hydroxylamine monohydrate; tetrabutyl ammonium fluoride; ethylamine; copper(l) chloride;
In
tetrahydrofuran; methanol; hexane;
DOI:10.1021/ja1071916