3,3'-dichloro-2,2',4,4',5,5',6,6'-octafluorodiphenyl diselenide

Base Information

Chemical Name:3,3'-dichloro-2,2',4,4',5,5',6,6'-octafluorodiphenyl diselenide
CAS No.:1258626-44-6
Molecular Formula:C₁₂Cl₂F₈Se₂
Molecular Weight:524.945
Hs Code.:

Synonyms:3,3'-dichloro-2,2',4,4',5,5',6,6'-octafluorodiphenyl diselenide

Suppliers and Price of 3,3'-dichloro-2,2',4,4',5,5',6,6'-octafluorodiphenyl diselenide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,3'-dichloro-2,2',4,4',5,5',6,6'-octafluorodiphenyl diselenide

Chemical Property:

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Technology Process of 3,3'-dichloro-2,2',4,4',5,5',6,6'-octafluorodiphenyl diselenide

There total 1 articles about 3,3'-dichloro-2,2',4,4',5,5',6,6'-octafluorodiphenyl diselenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 5172-06-5
1-chloro-2,3,4,6-tetrafluorobenzene

: 1258626-44-6
3,3'-dichloro-2,2',4,4',5,5',6,6'-octafluorodiphenyl diselenide

Guidance literature:: 1-chloro-2,3,4,6-tetrafluorobenzene; With n-butyllithium; In diethyl ether; hexane; at -60 ℃; for 1.25h; Inert atmosphere;

With selenium; In diethyl ether; hexane; at -60 ℃; for 1h; Inert atmosphere;

With iodine; In diethyl ether; hexane; at -20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/ejic.201000607

Reference yield: 69.0%

: 1258626-44-6
3,3'-dichloro-2,2',4,4',5,5',6,6'-octafluorodiphenyl diselenide

: 1258626-46-8
3-chloro-2,4,5,6-tetrafluorophenylselenenyl chloride

Guidance literature:: With chlorine; In tetrachloromethane;
DOI:10.1002/ejic.201000607

Reference yield:

: 1258626-44-6
3,3'-dichloro-2,2',4,4',5,5',6,6'-octafluorodiphenyl diselenide

: 1258866-41-9
1,5-bis(3-chloro-2,4,5,6-tetrafluorophenyl)-2,4-diaza-1,5-diselena-3-thia-2,3-pentadiene

Guidance literature:: Multi-step reaction with 2 steps

1: chlorine / tetrachloromethane

2: N,N'-bis(trimethylsilyl)sulfurdiimide / hexane / -30 - 20 °C / Inert atmosphere

With N,N'-bis(trimethylsilyl)sulfurdiimide; chlorine; In tetrachloromethane; hexane;
DOI:10.1002/ejic.201000607