C₂₉H₃₅BrN₂O₃

Base Information

Chemical Name:C₂₉H₃₅BrN₂O₃
CAS No.:1447766-92-8
Molecular Formula:C₂₉H₃₅BrN₂O₃
Molecular Weight:539.512
Hs Code.:

C<sub>29</sub>H<sub>35</sub>BrN<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₉H₃₅BrN₂O₃

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Chemical Property of C₂₉H₃₅BrN₂O₃

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Technology Process of C₂₉H₃₅BrN₂O₃

There total 5 articles about C₂₉H₃₅BrN₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₃₄BrN₂O₃⁽¹⁺⁾*I^(1-)

: 1447766-92-8
C₂₉H₃₅BrN₂O₃

Guidance literature:: With acetic acid; zinc; In tetrahydrofuran; at 20 ℃; for 25h; Inert atmosphere;
DOI:10.1021/ja405548b

Reference yield:

: C₂₂H₂₂BrNO₂

: 1447766-92-8
C₂₉H₃₅BrN₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 1 h / -78 °C / Inert atmosphere

1.2: 2.5 h / -78 - 20 °C / Inert atmosphere

2.1: L-proline / dichloromethane; acetonitrile / 216 h / Inert atmosphere

3.1: sodium hydride / mineral oil; dimethyl sulfoxide / 0.75 h / Inert atmosphere

3.2: 30 h / 20 °C / Inert atmosphere

4.1: sodium iodide; chloro-trimethyl-silane / tetrahydrofuran; acetonitrile / 2 h / Inert atmosphere

5.1: acetic acid; zinc / tetrahydrofuran / 25 h / 20 °C / Inert atmosphere

With chloro-trimethyl-silane; oxalyl dichloride; sodium hydride; acetic acid; dimethyl sulfoxide; L-proline; sodium iodide; zinc; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; acetonitrile; mineral oil; 1.1: |Swern Oxidation;
DOI:10.1021/ja405548b

Reference yield:

: 1447766-82-6
C₂₈H₃₁BrN₂O₃

: 1447766-92-8
C₂₉H₃₅BrN₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / mineral oil; dimethyl sulfoxide / 0.75 h / Inert atmosphere

1.2: 30 h / 20 °C / Inert atmosphere

2.1: sodium iodide; chloro-trimethyl-silane / tetrahydrofuran; acetonitrile / 2 h / Inert atmosphere

3.1: acetic acid; zinc / tetrahydrofuran / 25 h / 20 °C / Inert atmosphere

With chloro-trimethyl-silane; sodium hydride; acetic acid; sodium iodide; zinc; In tetrahydrofuran; dimethyl sulfoxide; acetonitrile; mineral oil;
DOI:10.1021/ja405548b