αH-4-(2-(alaninocarbonyl)ethyl)tetradecachlorotriphenylmethane ethyl ester

Base Information

Chemical Name:αH-4-(2-(alaninocarbonyl)ethyl)tetradecachlorotriphenylmethane ethyl ester
CAS No.:101981-03-7
Molecular Formula:C₂₇H₁₅Cl₁₄NO₃
Molecular Weight:897.763
Hs Code.:

Synonyms:αH-4-(2-(alaninocarbonyl)ethyl)tetradecachlorotriphenylmethane ethyl ester

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Chemical Property of αH-4-(2-(alaninocarbonyl)ethyl)tetradecachlorotriphenylmethane ethyl ester

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Technology Process of αH-4-(2-(alaninocarbonyl)ethyl)tetradecachlorotriphenylmethane ethyl ester

There total 7 articles about αH-4-(2-(alaninocarbonyl)ethyl)tetradecachlorotriphenylmethane ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1115-59-9
(S)-alanine ethyl ester hydrochloride

: 101981-01-5
αH-4-(2-carboxyethyl)tetradecachlorotriphenylmethane

: 101981-03-7
αH-4-(2-(alaninocarbonyl)ethyl)tetradecachlorotriphenylmethane ethyl ester

Guidance literature:: With triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; for 4h; Ambient temperature;
DOI:10.1021/jo00363a013

Reference yield:

: 79839-38-6
6,6’-((2,3,5,6-tetrachloro-4-methylphenyl)methylene)bis(1,2,3,4,5-pentachlorobenzene)

: 101981-03-7
αH-4-(2-(alaninocarbonyl)ethyl)tetradecachlorotriphenylmethane ethyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 95 percent / Br₂ / CCl₄ / 5 h / Irradiation

2: 82 percent / acetic acid / 72 h / Heating

3: 85 percent / aq. concd HCl / dioxane / 21 h / Heating

4: 87 percent / aq. NaOH / dioxane / 35 h / Ambient temperature

5: 83 percent / K₂CO₃ / dioxane / 20 h / Heating

6: 83 percent / aq. concd HCl / dioxane / 48 h / Heating

7: 51 percent / dicyclohexylcarbodiimide, triethylamine / CH₂Cl₂ / 4 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; bromine; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane; tetrachloromethane; dichloromethane; acetic acid;
DOI:10.1021/jo00363a013

Reference yield:

: 101998-20-3
6,6'-((4-(bromomethyl)-2,3,5,6-tetrachlorophenyl)methylene)bis(1,2,3,4,5-pentachlorobenzene)

: 101981-03-7
αH-4-(2-(alaninocarbonyl)ethyl)tetradecachlorotriphenylmethane ethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 82 percent / acetic acid / 72 h / Heating

2: 85 percent / aq. concd HCl / dioxane / 21 h / Heating

3: 87 percent / aq. NaOH / dioxane / 35 h / Ambient temperature

4: 83 percent / K₂CO₃ / dioxane / 20 h / Heating

5: 83 percent / aq. concd HCl / dioxane / 48 h / Heating

6: 51 percent / dicyclohexylcarbodiimide, triethylamine / CH₂Cl₂ / 4 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane; acetic acid;
DOI:10.1021/jo00363a013