benzyl 2-deoxy-4,6-O-isopropylidene-2-<(3R)-3-tetradecanoyloxytetradecanamido>-3-O-<(3R)-3-tetradecanoyloxytetradecanoyl>-β-D-glucopyranoside

Base Information

Chemical Name:benzyl 2-deoxy-4,6-O-isopropylidene-2-<(3R)-3-tetradecanoyloxytetradecanamido>-3-O-<(3R)-3-tetradecanoyloxytetradecanoyl>-β-D-glucopyranoside
CAS No.:111247-07-5
Molecular Formula:C₇₂H₁₂₇NO₁₁
Molecular Weight:1182.8
Hs Code.:

benzyl 2-deoxy-4,6-O-isopropylidene-2-<(3R)-3-tetradecanoyloxytetradecanamido>-3-O-<(3R)-3-tetradecanoyloxytetradecanoyl>-β-D-glucopyranoside

Synonyms:benzyl 2-deoxy-4,6-O-isopropylidene-2-<(3R)-3-tetradecanoyloxytetradecanamido>-3-O-<(3R)-3-tetradecanoyloxytetradecanoyl>-β-D-glucopyranoside

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Chemical Property of benzyl 2-deoxy-4,6-O-isopropylidene-2-<(3R)-3-tetradecanoyloxytetradecanamido>-3-O-<(3R)-3-tetradecanoyloxytetradecanoyl>-β-D-glucopyranoside

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Technology Process of benzyl 2-deoxy-4,6-O-isopropylidene-2-<(3R)-3-tetradecanoyloxytetradecanamido>-3-O-<(3R)-3-tetradecanoyloxytetradecanoyl>-β-D-glucopyranoside

There total 7 articles about benzyl 2-deoxy-4,6-O-isopropylidene-2-<(3R)-3-tetradecanoyloxytetradecanamido>-3-O-<(3R)-3-tetradecanoyloxytetradecanoyl>-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 87357-76-4
(R)-3-(dodecanoyloxy)tetradecanoic acid

: 111247-06-4
benzyl 2-deoxy-4,6-O-isopropylidene-2-<(3R)-3-tetradecanoyloxytetradecanamido>-β-D-glucopyranoside

: 111247-07-5
benzyl 2-deoxy-4,6-O-isopropylidene-2-<(3R)-3-tetradecanoyloxytetradecanamido>-3-O-<(3R)-3-tetradecanoyloxytetradecanoyl>-β-D-glucopyranoside

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; Ambient temperature;
DOI:10.1016/0008-6215(87)80207-0

Reference yield:

: 87357-65-1
(3R)-3-hydroxytetradecanoic acid phenacyl ester

: 111247-07-5
benzyl 2-deoxy-4,6-O-isopropylidene-2-<(3R)-3-tetradecanoyloxytetradecanamido>-3-O-<(3R)-3-tetradecanoyloxytetradecanoyl>-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / pyridine / 4-(dimethylamino)pyridine

2: zinc dust / acetic acid / 50 °C

3: 91 percent / DCC / CH₂Cl₂ / 4.5 h / Ambient temperature

4: 81 percent / DCC, DMAP / CH₂Cl₂ / Ambient temperature

With pyridine; dmap; dicyclohexyl-carbodiimide; zinc; dmap; In dichloromethane; acetic acid;
DOI:10.1016/0008-6215(87)80207-0

Reference yield:

: 28715-21-1,3422-31-9
(R)-3-hydroxytetradecanoic acid

: 111247-07-5
benzyl 2-deoxy-4,6-O-isopropylidene-2-<(3R)-3-tetradecanoyloxytetradecanamido>-3-O-<(3R)-3-tetradecanoyloxytetradecanoyl>-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / ethyl acetate / 6 h / Ambient temperature

2: 90 percent / pyridine / 4-(dimethylamino)pyridine

3: zinc dust / acetic acid / 50 °C

4: 91 percent / DCC / CH₂Cl₂ / 4.5 h / Ambient temperature

5: 81 percent / DCC, DMAP / CH₂Cl₂ / Ambient temperature

With pyridine; dmap; triethylamine; dicyclohexyl-carbodiimide; zinc; dmap; In dichloromethane; acetic acid; ethyl acetate;
DOI:10.1016/0008-6215(87)80207-0