Technology Process of 2-(4-methyl-3-pentylphenyl)ethanol
There total 7 articles about 2-(4-methyl-3-pentylphenyl)ethanol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium 10% on activated carbon;
In
ethanol;
at 40 ℃;
for 5h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium hydroxide; tetrabutylammomium bromide / tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 4 h / Reflux; Inert atmosphere
2: hydrogen / palladium 10% on activated carbon / ethanol / 5 h / 40 °C
With
tetrabutylammomium bromide; hydrogen; potassium hydroxide;
tetrakis(triphenylphosphine) palladium(0); palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sulfur / toluene-4-sulfonic acid / 7 h / 130 °C / Inert atmosphere
2.1: sodium hydroxide; water / ethanol / 4 h / Reflux
3.1: hydrogenchloride / 3.5 h / Reflux
4.1: dimethylsulfide; borane / tetrahydrofuran / 3 h / Inert atmosphere; Reflux
4.2: 0.5 h / 0 °C / Reflux
5.1: potassium hydroxide; tetrabutylammomium bromide / tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 4 h / Reflux; Inert atmosphere
6.1: hydrogen / palladium 10% on activated carbon / ethanol / 5 h / 40 °C
With
hydrogenchloride; dimethylsulfide; borane; tetrabutylammomium bromide; water; hydrogen; sulfur; potassium hydroxide; sodium hydroxide;
tetrakis(triphenylphosphine) palladium(0); palladium 10% on activated carbon; toluene-4-sulfonic acid;
In
tetrahydrofuran; ethanol;