C₂₉H₄₁NO₃

Base Information

Chemical Name:C₂₉H₄₁NO₃
CAS No.:944027-71-8
Molecular Formula:C₂₉H₄₁NO₃
Molecular Weight:451.649
Hs Code.:

C<sub>29</sub>H<sub>41</sub>NO<sub>3</sub>

Synonyms:C₂₉H₄₁NO₃

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Chemical Property of C₂₉H₄₁NO₃

Chemical Property:

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Technology Process of C₂₉H₄₁NO₃

There total 6 articles about C₂₉H₄₁NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 944027-66-1
C₃₈H₆₁NO₃Si

: 944027-71-8
C₂₉H₄₁NO₃

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1021/ja0718873

Reference yield:

: 464-49-3,68546-28-1
(1R,4R)-1,7,7-trimethylbicyclo[2.2.1]heptan-2-one

: 944027-71-8
C₂₉H₄₁NO₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: 85 percent / m-CPBA; trifluoromethanesulfonic acid / CH₂Cl₂ / 3 h / 20 °C

2.1: 91 percent / Dibal-H / toluene / 2.5 h / -78 °C

3.1: 8.70 mg / aq. NaOH / tetra-n-butylammonium hydrogensulfate / CH₂Cl₂; toluene / 6 h / 0 - 20 °C

4.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

4.2: 86 percent / tetrahydrofuran; hexane / -78 - 20 °C

5.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

5.2: 86 percent / tetrahydrofuran; hexane / 1 h / -78 °C

6.1: 60 percent / Florisil / 20 °C

7.1: 92 percent / tetra-n-butylammonium fluoride trihydrate / tetrahydrofuran / 0.5 h / 20 °C

With sodium hydroxide; florisil; n-butyllithium; trifluorormethanesulfonic acid; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; 3-chloro-benzenecarboperoxoic acid; tetra(n-butyl)ammonium hydrogensulfate; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1021/ja0718873

Reference yield:

: 30860-35-6
(1R,5S)-1,8,8-trimethyl-3-oxabicyclo[3.2.1]octan-2-one

: 944027-71-8
C₂₉H₄₁NO₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: 91 percent / Dibal-H / toluene / 2.5 h / -78 °C

2.1: 8.70 mg / aq. NaOH / tetra-n-butylammonium hydrogensulfate / CH₂Cl₂; toluene / 6 h / 0 - 20 °C

3.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

3.2: 86 percent / tetrahydrofuran; hexane / -78 - 20 °C

4.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

4.2: 86 percent / tetrahydrofuran; hexane / 1 h / -78 °C

5.1: 60 percent / Florisil / 20 °C

6.1: 92 percent / tetra-n-butylammonium fluoride trihydrate / tetrahydrofuran / 0.5 h / 20 °C

With sodium hydroxide; florisil; n-butyllithium; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; tetra(n-butyl)ammonium hydrogensulfate; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1021/ja0718873