1-<3-propyl>-4-<(4-chlorophenyl)amino>-4-piperidinecarboxamide

Base Information

Chemical Name:1-<3-propyl>-4-<(4-chlorophenyl)amino>-4-piperidinecarboxamide
CAS No.:97861-28-4
Molecular Formula:C₂₇H₂₉ClF₂N₄O
Molecular Weight:499.003
Hs Code.:

1-<3-<bis(4-fluorophenyl)amino>propyl>-4-<(4-chlorophenyl)amino>-4-piperidinecarboxamide

Synonyms:1-<3-propyl>-4-<(4-chlorophenyl)amino>-4-piperidinecarboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<3-propyl>-4-<(4-chlorophenyl)amino>-4-piperidinecarboxamide

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Technology Process of 1-<3-propyl>-4-<(4-chlorophenyl)amino>-4-piperidinecarboxamide

There total 4 articles about 1-<3-propyl>-4-<(4-chlorophenyl)amino>-4-piperidinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 97861-26-2
1-<3-propyl>-4-<(4-chlorophenyl)amino>-4-piperidinecarbonitrile

: 97861-28-4
1-<3-propyl>-4-<(4-chlorophenyl)amino>-4-piperidinecarboxamide

Guidance literature:: With sulfuric acid; at 25 ℃; for 24h;
DOI:10.1021/jm00150a011

Reference yield:

: 41979-39-9
4-piperidone hydrochloride

: 97861-28-4
1-<3-propyl>-4-<(4-chlorophenyl)amino>-4-piperidinecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / sodium carbonate, sodium iodide / dimethylformamide / 20 h / 75 - 90 °C

2: 1.) toluene, reflux, 2.5 h, 2.) toluene, 50 deg C

3: 85 percent / conc. sulfuric acid / 24 h / 25 °C

With sulfuric acid; sodium carbonate; sodium iodide; In N,N-dimethyl-formamide;
DOI:10.1021/jm00150a011

Reference yield:

: 80119-31-9
N-(3-chloropropyl)-4-fluoro-N-(4-fluorophenyl)benzenamine

: 97861-28-4
1-<3-propyl>-4-<(4-chlorophenyl)amino>-4-piperidinecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / sodium carbonate, sodium iodide / dimethylformamide / 20 h / 75 - 90 °C

2: 1.) toluene, reflux, 2.5 h, 2.) toluene, 50 deg C

3: 85 percent / conc. sulfuric acid / 24 h / 25 °C

With sulfuric acid; sodium carbonate; sodium iodide; In N,N-dimethyl-formamide;
DOI:10.1021/jm00150a011