3-Ethoxy-6-(methylthio)-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidin-4(5H)-one

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Chemical Name:3-Ethoxy-6-(methylthio)-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidin-4(5H)-one
CAS No.:111375-34-9
Molecular Formula:C₃₄H₃₀N₄O₉S
Molecular Weight:670.7
Hs Code.:

Synonyms:3-Ethoxy-6-(methylthio)-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidin-4(5H)-one

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Chemical Property of 3-Ethoxy-6-(methylthio)-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidin-4(5H)-one

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Technology Process of 3-Ethoxy-6-(methylthio)-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidin-4(5H)-one

There total 4 articles about 3-Ethoxy-6-(methylthio)-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidin-4(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 6974-32-9
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

: 111375-38-3
3-Ethoxy-6-(methylthio)pyrazolo<3,4-d>pyrimidin-4(5H)-one

: 111375-34-9
3-Ethoxy-6-(methylthio)-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidin-4(5H)-one

Guidance literature:: With boron trifluoride diethyl etherate; In nitromethane; for 3h; Heating;
DOI:10.1002/jhet.5570230651

Reference yield:

: 111375-37-2
3-Ethoxy-6-thioxopyrazolo<3,4-d>pyrimidin-4(5H,7H)-one

: 111375-34-9
3-Ethoxy-6-(methylthio)-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidin-4(5H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / aq. 1N NaOH / 18 h / Ambient temperature

2: 61 percent / BF₃*(C₂H₅)2O / nitromethane / 3 h / Heating

With sodium hydroxide; boron trifluoride diethyl etherate; In nitromethane;
DOI:10.1002/jhet.5570230651

Reference yield:

: 111375-26-9
5-amino-3-ethoxy-1H-pyrazole-4-carbonitrile

: 111375-34-9
3-Ethoxy-6-(methylthio)-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidin-4(5H)-one

Guidance literature:: Multi-step reaction with 4 steps

1: 79 percent / conc. H₂SO₄ / 1 h / Ambient temperature

2: 2.) aq. 2N NaOH; / 1.) dimethyl formamide, reflux, 3 h, 2.) 70 deg C;

3: 74 percent / aq. 1N NaOH / 18 h / Ambient temperature

4: 61 percent / BF₃*(C₂H₅)2O / nitromethane / 3 h / Heating

With sodium hydroxide; sulfuric acid; boron trifluoride diethyl etherate; In nitromethane;
DOI:10.1002/jhet.5570230651