4-phenyl-4-((4-carboethoxymethylpiperazin-1-yl)carboxamido)piperidine hydriodic acid salt

Base Information

Chemical Name:4-phenyl-4-((4-carboethoxymethylpiperazin-1-yl)carboxamido)piperidine hydriodic acid salt
CAS No.:209667-52-7
Molecular Formula:C₂₀H₂₉N₃O₃*HI
Molecular Weight:487.381
Hs Code.:

Synonyms:4-phenyl-4-((4-carboethoxymethylpiperazin-1-yl)carboxamido)piperidine hydriodic acid salt

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Chemical Property of 4-phenyl-4-((4-carboethoxymethylpiperazin-1-yl)carboxamido)piperidine hydriodic acid salt

Chemical Property:

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Technology Process of 4-phenyl-4-((4-carboethoxymethylpiperazin-1-yl)carboxamido)piperidine hydriodic acid salt

There total 4 articles about 4-phenyl-4-((4-carboethoxymethylpiperazin-1-yl)carboxamido)piperidine hydriodic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 209667-67-4
1-t-butoxycarbonyl-4-phenyl-4-((4-carboethoxymethylpiperazin-1-yl)carboxamido)piperidine

: 209667-52-7
4-phenyl-4-((4-carboethoxymethylpiperazin-1-yl)carboxamido)piperidine hydriodic acid salt

Guidance literature:: With hydrogen iodide; In ethanol; water; for 21h; Heating / reflux;

Reference yield:

: 167262-68-2
N-(t-butyloxycarbonyl)-4-phenylpiperidine-4-carboxylic acid

: 209667-52-7
4-phenyl-4-((4-carboethoxymethylpiperazin-1-yl)carboxamido)piperidine hydriodic acid salt

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 h

2: hydrogen iodide / ethanol; water / 21 h / Heating / reflux

With hydrogen iodide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; water;

Reference yield:

: 4-phenyl-4-piperidinecarboxylic acid 4-methylbenzenesulfonate

: 209667-52-7
4-phenyl-4-((4-carboethoxymethylpiperazin-1-yl)carboxamido)piperidine hydriodic acid salt

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / DMF (N,N-dimethyl-formamide) / 20 h

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 h

3: hydrogen iodide / ethanol; water / 21 h / Heating / reflux

With hydrogen iodide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; water;