C₉₃H₁₁₈

Base Information

Chemical Name:C₉₃H₁₁₈
CAS No.:374082-21-0
Molecular Formula:C₉₃H₁₁₈
Molecular Weight:1235.96
Hs Code.:

Synonyms:C₉₃H₁₁₈

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₉₃H₁₁₈

Chemical Property:

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Technology Process of C₉₃H₁₁₈

There total 4 articles about C₉₃H₁₁₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105-06-6
1,4-Divinylbenzene

: 756877-81-3
C₈₃H₁₀₉Br

: 374082-21-0
C₉₃H₁₁₈

Guidance literature:: With palladium diacetate; tributyl-amine; tris-(o-tolyl)phosphine; In N,N-dimethyl-formamide; at 90 ℃; for 12h;
DOI:10.1021/ja0010812

Reference yield:

: 1-Bromo-2,5-dihexyl-4-((E)-2-p-tolyl-vinyl)-benzene

: 374082-21-0
C₉₃H₁₁₈

Guidance literature:: Multi-step reaction with 3 steps

1: tri-o-tolylphosphine; NBu₃; Pd(OAc)2 / dimethylformamide / 12 h / 90 °C

2: NaH / 1,2-dimethoxy-ethane / 5 h / Heating

3: tri-o-tolylphosphine; NBu₃; Pd(OAc)2 / dimethylformamide / 12 h / 90 °C

With palladium diacetate; tributyl-amine; sodium hydride; tris-(o-tolyl)phosphine; In 1,2-dimethoxyethane; N,N-dimethyl-formamide; 1: Heck reaction / 2: Wittig reaction / 3: Heck reaction;
DOI:10.1021/ja0010812

Reference yield:

: 2,5-Dihexyl-4-[(E)-2-(4-vinyl-phenyl)-vinyl]-benzaldehyde

: 374082-21-0
C₉₃H₁₁₈

Guidance literature:: Multi-step reaction with 3 steps

1: tri-o-tolylphosphine; NBu₃; Pd(OAc)2 / dimethylformamide / 12 h / 90 °C

2: NaH / 1,2-dimethoxy-ethane / 5 h / Heating

3: tri-o-tolylphosphine; NBu₃; Pd(OAc)2 / dimethylformamide / 12 h / 90 °C

With palladium diacetate; tributyl-amine; sodium hydride; tris-(o-tolyl)phosphine; In 1,2-dimethoxyethane; N,N-dimethyl-formamide; 1: Heck reaction / 2: Wittig reaction / 3: Heck reaction;
DOI:10.1021/ja0010812