10-hexyl-3,7-bis(7-phenylbenzo[c][1,2,5]thiadiazol-4-yl)-10H-phenothiazine

Base Information

Chemical Name:10-hexyl-3,7-bis(7-phenylbenzo[c][1,2,5]thiadiazol-4-yl)-10H-phenothiazine
CAS No.:1579282-49-7
Molecular Formula:C₄₂H₃₃N₅S₃
Molecular Weight:703.956
Hs Code.:

Synonyms:10-hexyl-3,7-bis(7-phenylbenzo[c][1,2,5]thiadiazol-4-yl)-10H-phenothiazine

Suppliers and Price of 10-hexyl-3,7-bis(7-phenylbenzo[c][1,2,5]thiadiazol-4-yl)-10H-phenothiazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 10-hexyl-3,7-bis(7-phenylbenzo[c][1,2,5]thiadiazol-4-yl)-10H-phenothiazine

Chemical Property:

Purity/Quality:: 98%+ ^*data from raw suppliers

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Technology Process of 10-hexyl-3,7-bis(7-phenylbenzo[c][1,2,5]thiadiazol-4-yl)-10H-phenothiazine

There total 2 articles about 10-hexyl-3,7-bis(7-phenylbenzo[c][1,2,5]thiadiazol-4-yl)-10H-phenothiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: (4-bromo-7-phenylbenzo[c][1,2,5]thiadiazole)

: 405198-30-3
10-hexyl-3,7-bis(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)-10H-phenothiazine

: 1579282-49-7
10-hexyl-3,7-bis(7-phenylbenzo[c][1,2,5]thiadiazol-4-yl)-10H-phenothiazine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In water; toluene; at 85 - 90 ℃; for 48h;
DOI:10.1002/anie.201308486

Reference yield:

: 312924-93-9
3,7-dibromo-10-hexyl-10H-phenothiazine

: 1579282-49-7
10-hexyl-3,7-bis(7-phenylbenzo[c][1,2,5]thiadiazol-4-yl)-10H-phenothiazine

Guidance literature:: Multi-step reaction with 2 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 24 h / 85 °C

2: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / 48 h / 85 - 90 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; sodium carbonate; In 1,4-dioxane; water; toluene;
DOI:10.1002/anie.201308486