Technology Process of Gossylic nitrile-1,1'-diacetate
There total 4 articles about Gossylic nitrile-1,1'-diacetate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
water; potassium carbonate;
In
methanol;
for 0.5h;
Heating;
DOI:10.1021/jm00159a043
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 5 h / Ambient temperature
2: acetic anhydride / 1.) RT, 2 h, 2.) from RT to reflux, 60 min
3: 71 percent / acetic anhydride / 0.5 h / Heating
4: 71 percent / H2O, K2CO3 / methanol / 0.5 h / Heating
With
water; acetic anhydride; potassium carbonate;
In
methanol;
DOI:10.1021/jm00159a043
- Guidance literature:
-
Multi-step reaction with 3 steps
1: acetic anhydride / 1.) RT, 2 h, 2.) from RT to reflux, 60 min
2: 71 percent / acetic anhydride / 0.5 h / Heating
3: 71 percent / H2O, K2CO3 / methanol / 0.5 h / Heating
With
water; acetic anhydride; potassium carbonate;
In
methanol;
DOI:10.1021/jm00159a043
