Technology Process of Gossylic nitrile-1,1'-diacetate
There total 4 articles about Gossylic nitrile-1,1'-diacetate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; potassium carbonate;
In
methanol;
for 0.5h;
Heating;
DOI:10.1021/jm00159a043
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 5 h / Ambient temperature
2: acetic anhydride / 1.) RT, 2 h, 2.) from RT to reflux, 60 min
3: 71 percent / acetic anhydride / 0.5 h / Heating
4: 71 percent / H2O, K2CO3 / methanol / 0.5 h / Heating
With
water; acetic anhydride; potassium carbonate;
In
methanol;
DOI:10.1021/jm00159a043
- Guidance literature:
-
Multi-step reaction with 3 steps
1: acetic anhydride / 1.) RT, 2 h, 2.) from RT to reflux, 60 min
2: 71 percent / acetic anhydride / 0.5 h / Heating
3: 71 percent / H2O, K2CO3 / methanol / 0.5 h / Heating
With
water; acetic anhydride; potassium carbonate;
In
methanol;
DOI:10.1021/jm00159a043