(1S,2R,5S)-5-methyl-2-(1-methylethyl)cyclohexyl diethoxyphosphorylacetate

Base Information

Chemical Name:(1S,2R,5S)-5-methyl-2-(1-methylethyl)cyclohexyl diethoxyphosphorylacetate
CAS No.:217823-21-7
Molecular Formula:C₁₆H₃₁O₅P
Molecular Weight:334.393
Hs Code.:

Synonyms:(1S,2R,5S)-5-methyl-2-(1-methylethyl)cyclohexyl diethoxyphosphorylacetate

Suppliers and Price of (1S,2R,5S)-5-methyl-2-(1-methylethyl)cyclohexyl diethoxyphosphorylacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1S,2R,5S)-5-methyl-2-(1-methylethyl)cyclohexyl diethoxyphosphorylacetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1S,2R,5S)-5-methyl-2-(1-methylethyl)cyclohexyl diethoxyphosphorylacetate

There total 3 articles about (1S,2R,5S)-5-methyl-2-(1-methylethyl)cyclohexyl diethoxyphosphorylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 32815-12-6
(1S,2R,5S)-5-methyl-2-(1-methylethyl)cyclohexyl bromoacetate

: 122-52-1
triethyl phosphite

: 217823-21-7
(1S,2R,5S)-5-methyl-2-(1-methylethyl)cyclohexyl diethoxyphosphorylacetate

Guidance literature:: at 110 ℃; for 4h;

Reference yield: 97.0%

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 15356-60-2
(1S,2R,5S)-(+)-menthol

: 217823-21-7
(1S,2R,5S)-5-methyl-2-(1-methylethyl)cyclohexyl diethoxyphosphorylacetate

Guidance literature:: With dmap; In toluene; for 27h; Reflux; Inert atmosphere;
DOI:10.1002/ejoc.201100400

Reference yield:

: 15356-60-2
(1S,2R,5S)-(+)-menthol

: 217823-21-7
(1S,2R,5S)-5-methyl-2-(1-methylethyl)cyclohexyl diethoxyphosphorylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) toluene, RT, 1 h, 2.) toluene, RT, 3 h

2: 100 percent / 4 h / 110 °C

With sodium hydride;