1-(4-(benzyloxybenzoyl)phenyl)-2-(3,4,5-trimethoxyphenyl)-ortho-carborane

Base Information

Chemical Name:1-(4-(benzyloxybenzoyl)phenyl)-2-(3,4,5-trimethoxyphenyl)-ortho-carborane
CAS No.:1580436-07-2
Molecular Formula:C₃₁H₃₆B₁₀O₅
Molecular Weight:596.734
Hs Code.:

Synonyms:1-(4-(benzyloxybenzoyl)phenyl)-2-(3,4,5-trimethoxyphenyl)-ortho-carborane

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Chemical Property of 1-(4-(benzyloxybenzoyl)phenyl)-2-(3,4,5-trimethoxyphenyl)-ortho-carborane

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Technology Process of 1-(4-(benzyloxybenzoyl)phenyl)-2-(3,4,5-trimethoxyphenyl)-ortho-carborane

There total 3 articles about 1-(4-(benzyloxybenzoyl)phenyl)-2-(3,4,5-trimethoxyphenyl)-ortho-carborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17702-41-9
nido-decaborane

: 1580436-06-1
C₂₀H₁₅IO₂

: 185698-55-9
2-(3-hydroxy-4-methoxyphenyl)-1-(3',4',5'-trimethoxyphenyl)ethyne

: 1580436-07-2
1-(4-(benzyloxybenzoyl)phenyl)-2-(3,4,5-trimethoxyphenyl)-ortho-carborane

Guidance literature:: C₂₀H₁₅IO₂; 2-(3"-hydroxy-4"-methoxyphenyl)-1-(3',4',5'-trimethoxyphenyl)ethyne; With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; for 4h; Reflux;

nido-decaborane; With N,N-dimethyl-aniline; In chlorobenzene; at 120 ℃; for 0.25h; Microwave irradiation;
DOI:10.1039/c3dt52828f

Reference yield:

: 53560-33-1
3,4,5-trimethoxyphenylacetylene

: 1580436-07-2
1-(4-(benzyloxybenzoyl)phenyl)-2-(3,4,5-trimethoxyphenyl)-ortho-carborane

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / tetrahydrofuran / 4 - 6 h / Reflux

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / tetrahydrofuran / 4 h / Reflux

2.2: 0.25 h / 120 °C / Microwave irradiation

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1.1: |Sonogashira Cross-Coupling / 2.1: |Sonogashira Cross-Coupling;
DOI:10.1039/c3dt52828f

Reference yield:

: 210967-30-9
C₂₀H₁₇NO₂

: 1580436-07-2
1-(4-(benzyloxybenzoyl)phenyl)-2-(3,4,5-trimethoxyphenyl)-ortho-carborane

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite; potassium iodide / acetonitrile / 5 h / 0 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / tetrahydrofuran / 4 h / Reflux

2.2: 0.25 h / 120 °C / Microwave irradiation

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium iodide; sodium nitrite; In tetrahydrofuran; acetonitrile; 2.1: |Sonogashira Cross-Coupling;
DOI:10.1039/c3dt52828f