2-iodo-9,10-diphenylanthracene

Base Information

Chemical Name:2-iodo-9,10-diphenylanthracene
CAS No.:1123921-69-6
Molecular Formula:C₂₆H₁₇I
Molecular Weight:456.325
Hs Code.:

Synonyms:2-iodo-9,10-diphenylanthracene

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Chemical Property of 2-iodo-9,10-diphenylanthracene

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Technology Process of 2-iodo-9,10-diphenylanthracene

There total 4 articles about 2-iodo-9,10-diphenylanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 2-iodo-9,10-diphenyl-9,10-epoxyanthracene

: 1123921-69-6
2-iodo-9,10-diphenylanthracene

Guidance literature:: With triethylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h; Reagent/catalyst; Inert atmosphere; Sealed tube;
DOI:10.1055/s-0036-1591510

Reference yield:

: 572-83-8
2-bromoanthracene-9,10-dione

: 1123921-69-6
2-iodo-9,10-diphenylanthracene

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

2.1: potassium iodide; acetic acid; sodium hypophosphite monohydrate / 2 h / 120 °C

2.2: 1 h / 120 °C

3.1: n-butyllithium; sodium thiosulfate / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

3.2: 13 h / -78 - 20 °C

3.3: 1 h / 20 °C

With n-butyllithium; sodium hypophosphite monohydrate; sodium thiosulfate; acetic acid; potassium iodide; In tetrahydrofuran;

Reference yield:

: 117-79-3
2-aminoanthraquinone

: 1123921-69-6
2-iodo-9,10-diphenylanthracene

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(ll) bromide; tert.-butylnitrite / acetonitrile / 6 h / 65 °C

1.2: 3 h

2.1: tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

3.1: potassium iodide; acetic acid; sodium hypophosphite monohydrate / 2 h / 120 °C

3.2: 1 h / 120 °C

4.1: n-butyllithium; sodium thiosulfate / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

4.2: 13 h / -78 - 20 °C

4.3: 1 h / 20 °C

With n-butyllithium; tert.-butylnitrite; sodium hypophosphite monohydrate; sodium thiosulfate; acetic acid; potassium iodide; copper(ll) bromide; In tetrahydrofuran; acetonitrile;