5-[3-(4-allyloxy-3-chlorobenzyloxy)azetidin-1-yl]-5-methyl-2,2-diphenylhexanoic acid amide

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Chemical Name:5-[3-(4-allyloxy-3-chlorobenzyloxy)azetidin-1-yl]-5-methyl-2,2-diphenylhexanoic acid amide
CAS No.:931410-39-8
Molecular Formula:C₃₂H₃₇ClN₂O₃
Molecular Weight:533.11
Hs Code.:

Synonyms:5-[3-(4-allyloxy-3-chlorobenzyloxy)azetidin-1-yl]-5-methyl-2,2-diphenylhexanoic acid amide

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Chemical Property of 5-[3-(4-allyloxy-3-chlorobenzyloxy)azetidin-1-yl]-5-methyl-2,2-diphenylhexanoic acid amide

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Technology Process of 5-[3-(4-allyloxy-3-chlorobenzyloxy)azetidin-1-yl]-5-methyl-2,2-diphenylhexanoic acid amide

There total 1 articles about 5-[3-(4-allyloxy-3-chlorobenzyloxy)azetidin-1-yl]-5-methyl-2,2-diphenylhexanoic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 20788-43-6
1-allyloxy-2-chloro-4-chloromethylbenzene

: 931410-39-8
5-[3-(4-allyloxy-3-chlorobenzyloxy)azetidin-1-yl]-5-methyl-2,2-diphenylhexanoic acid amide

Guidance literature:: 5-(3-hydroxyazetidin-1-yl)-5-methyl-2,2-diphenylhexanoic acid amide; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

1-allyloxy-2-chloro-4-chloromethylbenzene; In N,N-dimethyl-formamide; for 0.5h;

With hydrogenchloride; sodium hydrogencarbonate; more than 3 stages;

Reference yield: 38.0%

: 931410-39-8
5-[3-(4-allyloxy-3-chlorobenzyloxy)azetidin-1-yl]-5-methyl-2,2-diphenylhexanoic acid amide

: 5-[3-(3-chloro-4-hydroxybenzyloxy)azetidin-1-yl]-5-methyl-2,2-diphenylhexanoic acid amide

Guidance literature:: 5-[3-(4-allyloxy-3-chlorobenzyloxy)azetidin-1-yl]-5-methyl-2,2-diphenylhexanoic acid amide; With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 45 ℃; for 0.5h;

With acetic acid; In tetrahydrofuran; water; at 20 ℃;

With sodium hydrogencarbonate; In tetrahydrofuran; water;