12,13-((3'β,4'β)-tetrahydrocyclopenta[3',4',2]dioxathiole-2-oxide-2'α,5'α-diyl)-6-(4-methoxybenzyl)-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-5,7(6H)-dione

Base Information

Chemical Name:12,13-((3'β,4'β)-tetrahydrocyclopenta[3',4',2]dioxathiole-2-oxide-2'α,5'α-diyl)-6-(4-methoxybenzyl)-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-5,7(6H)-dione
CAS No.:865606-87-7
Molecular Formula:C₃₃H₂₃N₃O₆S
Molecular Weight:589.628
Hs Code.:

12,13-((3'β,4'β)-tetrahydrocyclopenta[3',4',2]dioxathiole-2-oxide-2'α,5'α-diyl)-6-(4-methoxybenzyl)-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-5,7(6H)-dione

Synonyms:12,13-((3'β,4'β)-tetrahydrocyclopenta[3',4',2]dioxathiole-2-oxide-2'α,5'α-diyl)-6-(4-methoxybenzyl)-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-5,7(6H)-dione

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Chemical Property of 12,13-((3'β,4'β)-tetrahydrocyclopenta[3',4',2]dioxathiole-2-oxide-2'α,5'α-diyl)-6-(4-methoxybenzyl)-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-5,7(6H)-dione

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Technology Process of 12,13-((3'β,4'β)-tetrahydrocyclopenta[3',4',2]dioxathiole-2-oxide-2'α,5'α-diyl)-6-(4-methoxybenzyl)-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-5,7(6H)-dione

There total 5 articles about 12,13-((3'β,4'β)-tetrahydrocyclopenta[3',4',2]dioxathiole-2-oxide-2'α,5'α-diyl)-6-(4-methoxybenzyl)-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-5,7(6H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 703405-34-9
12,13-(3'β,4'β-dihydroxycyclopentan-2'α,5'α-diyl)-6-(4-methoxybenzyl)-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-5,7(6H)-dione

: 865606-87-7
12,13-((3'β,4'β)-tetrahydrocyclopenta[3',4',2]dioxathiole-2-oxide-2'α,5'α-diyl)-6-(4-methoxybenzyl)-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-5,7(6H)-dione

Guidance literature:: With thionyl chloride; In tetrahydrofuran; for 18h; Heating;
DOI:10.1039/b506444a

Reference yield:

: 17040-70-9
cis-3,5-dibromocyclopentene

: 865606-87-7
12,13-((3'β,4'β)-tetrahydrocyclopenta[3',4',2]dioxathiole-2-oxide-2'α,5'α-diyl)-6-(4-methoxybenzyl)-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-5,7(6H)-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / dimethylformamide / 0.5 h

1.2: 73 percent / dimethylformamide

2.1: 95 percent / aq. OsO₄; NMMO / tetrahydrofuran; 2-methyl-propan-2-ol / 2 h

3.1: 98 percent / SOCl₂ / tetrahydrofuran / 18 h / Heating

With osmium(VIII) oxide; thionyl chloride; sodium hydride; 4-methylmorpholine N-oxide; In tetrahydrofuran; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1039/b506444a

Reference yield:

: 171824-53-6
C₂₈H₁₉N₃O₃

: 865606-87-7
12,13-((3'β,4'β)-tetrahydrocyclopenta[3',4',2]dioxathiole-2-oxide-2'α,5'α-diyl)-6-(4-methoxybenzyl)-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-5,7(6H)-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / dimethylformamide / 0.5 h

1.2: 73 percent / dimethylformamide

2.1: 95 percent / aq. OsO₄; NMMO / tetrahydrofuran; 2-methyl-propan-2-ol / 2 h

3.1: 98 percent / SOCl₂ / tetrahydrofuran / 18 h / Heating

With osmium(VIII) oxide; thionyl chloride; sodium hydride; 4-methylmorpholine N-oxide; In tetrahydrofuran; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1039/b506444a