C₁₆H₃₃NOSi

Base Information

• Chemical Name: C₁₆H₃₃NOSi
• CAS No.: 1093117-49-7
• Molecular Formula: C₁₆H₃₃NOSi
• Molecular Weight: 283.53
• Mol file: 1093117-49-7.mol

Synonyms:C₁₆H₃₃NOSi

Chemical Property of C₁₆H₃₃NOSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₆H₃₃NOSi

There total 1 articles about C₁₆H₃₃NOSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

1-chloro-N,N-diethyl-1,1-diisopropylsilanamine (147608-16-0) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → C16H33NOSi (1093117-49-7)

Guidance literature:

cyclohexanone; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

1-chloro-N,N-diethyl-1,1-diisopropylsilanamine; With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol802516z

Reference yield: 87.0%

C16H33NOSi (1093117-49-7) + C8H13O(1-)*Li(1+) → cyclohexenyloxy(5,5-dimethylcyclohex-1-enyloxy)diisopropylsilane (1093117-52-2)

Guidance literature:

C₁₆H₃₃NOSi; With Acetyl bromide; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

C₈H₁₃O^(1-)*Li⁽¹⁺⁾; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol802516z

Reference yield: 83.0%

C16H33NOSi (1093117-49-7) + lithium enolate of 1-tetralone (74074-96-7) → C22H32O2Si (1093117-51-1)

Guidance literature:

C₁₆H₃₃NOSi; With Acetyl bromide; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

lithium enolate of 1-tetralone; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol802516z

upstream raw materials:

1-chloro-N,N-diethyl-1,1-diisopropylsilanamine

cyclohexanone

Downstream raw materials:

cyclohexenyloxy(5,5-dimethylcyclohex-1-enyloxy)diisopropylsilane

(cyclohexenyloxy)(4,4-dimethylcyclohexa-1,5-dienyloxy)diisopropylsilane

C₂₂H₃₂O₂Si

(R)-cyclohexenyloxydiisopropyl(6-methyl-3-(prop-1-en-2-yl)cyclohexa-1,5-dienyloxy)silane