Technology Process of C23H33N3O2S
There total 6 articles about C23H33N3O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 15 h / 20 °C
2: triphenylphosphine / tetrahydrofuran; water
With
triethylamine; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; water;
2: Staudinger reduction;
DOI:10.1016/j.bmcl.2012.06.059
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium azide; tetrabutylammomium bromide; potassium iodide / toluene / Reflux
2.1: palladium on activated charcoal; hydrogen / ethanol / 20 °C
2.2: 2 h / 80 °C
2.3: 15 h / 20 °C
3.1: triethylamine / dichloromethane / 15 h / 20 °C
4.1: triphenylphosphine / tetrahydrofuran; water
With
sodium azide; palladium on activated charcoal; tetrabutylammomium bromide; hydrogen; triethylamine; triphenylphosphine; potassium iodide;
In
tetrahydrofuran; ethanol; dichloromethane; water; toluene;
4.1: Staudinger reduction;
DOI:10.1016/j.bmcl.2012.06.059