Technology Process of FNQ 3
There total 1 articles about FNQ 3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
benzene;
for 2h;
Heating;
DOI:10.1021/jm00394a013
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: selenium(IV) oxide; silica gel / dichloromethane / Microwave irradiation
2.1: acetic acid; dihydrogen peroxide / 1 h / 75 °C
3.1: quinoline; copper chromite / 2 h / Reflux
4.1: tetrabutylammomium bromide; potassium hydroxide; sodium dithionite / tetrahydrofuran / Inert atmosphere
5.1: n-butyllithium / tetrahydrofuran / -15 °C / Inert atmosphere
5.2: 20 °C / Inert atmosphere
6.1: water / acetonitrile / 0.33 h / 0 °C
6.2: 0.33 h
7.1: pyridine; zinc / 20 °C
With
pyridine; quinoline; selenium(IV) oxide; n-butyllithium; sodium dithionite; copper chromite; tetrabutylammomium bromide; water; dihydrogen peroxide; silica gel; acetic acid; potassium hydroxide; zinc;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jm3009597
- Guidance literature:
-
Multi-step reaction with 3 steps
1: selenium(IV) oxide; silica gel / dichloromethane / Microwave irradiation
2: acetic acid; dihydrogen peroxide / 1 h / 75 °C
3: dmap; dicyclohexyl-carbodiimide / 3 h / 0 - 20 °C
With
dmap; selenium(IV) oxide; dihydrogen peroxide; silica gel; acetic acid; dicyclohexyl-carbodiimide;
In
dichloromethane;
DOI:10.1021/jm3009597
