ethyl (1R,4R,5R,7S)-4-hydroxy-6-[(1R)-1-phenylethyl]-6-azabicyclo[3.2.1]octane-7-carboxylate

Base Information

Chemical Name:ethyl (1R,4R,5R,7S)-4-hydroxy-6-[(1R)-1-phenylethyl]-6-azabicyclo[3.2.1]octane-7-carboxylate
CAS No.:851390-24-4
Molecular Formula:C₁₈H₂₅NO₃
Molecular Weight:303.401
Hs Code.:

Synonyms:ethyl (1R,4R,5R,7S)-4-hydroxy-6-[(1R)-1-phenylethyl]-6-azabicyclo[3.2.1]octane-7-carboxylate

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Chemical Property of ethyl (1R,4R,5R,7S)-4-hydroxy-6-[(1R)-1-phenylethyl]-6-azabicyclo[3.2.1]octane-7-carboxylate

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Technology Process of ethyl (1R,4R,5R,7S)-4-hydroxy-6-[(1R)-1-phenylethyl]-6-azabicyclo[3.2.1]octane-7-carboxylate

There total 3 articles about ethyl (1R,4R,5R,7S)-4-hydroxy-6-[(1R)-1-phenylethyl]-6-azabicyclo[3.2.1]octane-7-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₂₄INO₃

: 851390-24-4
ethyl (1R,4R,5R,7S)-4-hydroxy-6-[(1R)-1-phenylethyl]-6-azabicyclo[3.2.1]octane-7-carboxylate

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 100 ℃; for 2h;

Reference yield:

: 134984-64-8
exo-2-aza-2-<(R)-1-phenylethyl>-3-ethoxycarbonyl<2.2.2>bicyclooct-5-ene

: 851390-24-4
ethyl (1R,4R,5R,7S)-4-hydroxy-6-[(1R)-1-phenylethyl]-6-azabicyclo[3.2.1]octane-7-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: N-iodo-succinimide; water / dimethyl sulfoxide / 3.5 h / 20 °C

2: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / 100 °C

With N-iodo-succinimide; 2,2'-azobis(isobutyronitrile); water; tri-n-butyl-tin hydride; In dimethyl sulfoxide; toluene;