Technology Process of cis-dichlorobis(3,3'-dimethyl-2,2'-bipyridine)rhodium(III) perchlorate - H2O (4/1)
There total 1 articles about cis-dichlorobis(3,3'-dimethyl-2,2'-bipyridine)rhodium(III) perchlorate - H2O (4/1) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
perchloric acid; hydrazine hydrate;
In
ethanol;
RhCl3*3H2O, ligand and cat. amounts of hydrazine hydrate in ethanol washeated at boiling for 5 min, filtered, HClO4 was added, the soln. was allowed to stand at room temp. for 20 min;; ppt. was filtered, washed with hot H2O (80°C), EtOH and ether, elem. anal.;;