(1,10-phenathroline)Pd(CH₂CH(CH₂CH₂CHCH₂)N-tosyl)

Base Information

Chemical Name:(1,10-phenathroline)Pd(CH₂CH(CH₂CH₂CHCH₂)N-tosyl)
CAS No.:918160-49-3
Molecular Formula:C₂₅H₂₅N₃O₂PdS
Molecular Weight:537.978
Hs Code.:

(1,10-phenathroline)Pd(CH<sub>2</sub>CH(CH<sub>2</sub>CH<sub>2</sub>CHCH<sub>2</sub>)N-tosyl)

Synonyms:(1,10-phenathroline)Pd(CH₂CH(CH₂CH₂CHCH₂)N-tosyl)

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Chemical Property of (1,10-phenathroline)Pd(CH₂CH(CH₂CH₂CHCH₂)N-tosyl)

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Technology Process of (1,10-phenathroline)Pd(CH₂CH(CH₂CH₂CHCH₂)N-tosyl)

There total 1 articles about (1,10-phenathroline)Pd(CH₂CH(CH₂CH₂CHCH₂)N-tosyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 66-71-7
1,10-Phenanthroline

: tris(dibenzylideneacetone)dipalladium ⁽⁰⁾

: 176516-06-6
2-but-3-enyl-1-(toluene-4-sulfonyl)aziridine

: 918160-49-3
(1,10-phenathroline)Pd(CH₂CH(CH₂CH₂CHCH₂)N-tosyl)

Guidance literature:: In tetrahydrofuran; under N2; THF added to mixt. of Pd complex and phenanthroline; stirred at room temp. for 1 min; soln. of aziridine in THF added; heated with stirring at 65°C for 5 h; cooled to room temp.; filtered under N2; filtrate concd. under reduced pressure; ether added; ppt. collected by vac. filtration; washed with ether and hexane; dried in vac.;
DOI:10.1021/ja0660756

Reference yield: 72.0%

: 918160-49-3
(1,10-phenathroline)Pd(CH₂CH(CH₂CH₂CHCH₂)N-tosyl)

: 918160-57-3
(1,10-phenathroline)Pd(CH₂CH(CH₂)CH₂CH₂CHN-tosyl)

Guidance literature:: copper(l) iodide; In dichloromethane; under N2; soln. of Pd complex in CH2Cl2 added to CuI (20 mol%); stirred at room temp. for 20 h; filtered under N2; filtrate concd. under reduced pressure; ether added; ppt. collected by vac. filtration; washed with ether and hexane; dried in vac.;
DOI:10.1021/ja0660756