C₄₄H₅₇N₃O₁₃S

Base Information

Chemical Name:C₄₄H₅₇N₃O₁₃S
CAS No.:141823-83-8
Molecular Formula:C₄₄H₅₇N₃O₁₃S
Molecular Weight:868.015
Hs Code.:

C<sub>44</sub>H<sub>57</sub>N<sub>3</sub>O<sub>13</sub>S

Synonyms:C₄₄H₅₇N₃O₁₃S

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Chemical Property of C₄₄H₅₇N₃O₁₃S

Chemical Property:

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Technology Process of C₄₄H₅₇N₃O₁₃S

There total 15 articles about C₄₄H₅₇N₃O₁₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 141823-82-7
C₄₄H₅₅N₃O₁₃S

: 141823-83-8
C₄₄H₅₇N₃O₁₃S

: 141900-21-2
C₄₄H₅₇N₃O₁₃S

Guidance literature:: With boron trifluoride diethyl etherate; sodium cyanoborohydride; In tetrahydrofuran; diethyl ether; dichloromethane; at -60 - -40 ℃; for 2h; Yield given. Yields of byproduct given;

Reference yield:

: 126900-87-6
3-Chloro-benzoic acid (2S,3R,6R)-2-aminooxy-4-(tert-butyl-dimethyl-silanyloxy)-6-methyl-3,6-dihydro-2H-pyran-3-yl ester

: 141823-83-8
C₄₄H₅₇N₃O₁₃S

Guidance literature:: Multi-step reaction with 10 steps

1: 70 percent / pyridinium p-toluenesulfonate / benzene / 3 h / 25 °C

2: 100 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h / 0 to 25 deg C

3: 95 percent / i-Bu₂AlH / CH₂Cl₂ / 0.5 h / -78 °C

4: 86 percent / acetonitrile / 1.5 h / 25 °C

5: 100 percent / toluene / 1 h / 100 °C

6: 95 percent / NaSMe, EtSH / CH₂Cl₂ / 1.5 h / 25 °C

7: 90 percent / i-Pr₂EtN / CH₂Cl₂ / 1 h / 25 °C

8: 1.) AcOH, n-Bu₄NF, 2.) K-Selectride / 1.) THF, -40 to 0 deg C, 2.) DME, THF, -78 deg C, 0.7 h

9: 85 percent / HF*py / CH₂Cl₂; tetrahydrofuran / 3 h / -20 - 0 °C

10: NaBH₃CN, BF₃*OEt₂ / CH₂Cl₂; tetrahydrofuran; diethyl ether / 2 h / -60 - -40 °C

With 2,6-dimethylpyridine; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; sodium cyanoborohydride; potassium tri-sec-butyl-borohydride; pyridine hydrogenfluoride; acetic acid; N-ethyl-N,N-diisopropylamine; ethanethiol; sodium thiomethoxide; In tetrahydrofuran; diethyl ether; dichloromethane; toluene; acetonitrile; benzene;

Reference yield:

: 132938-43-3
(3aS,4R,6R,7R,7aR)-7-Hydroxy-4-methyl-6-(2-nitro-benzyloxy)-tetrahydro-[1,3]dioxolo[4,5-c]pyran-2-one

: 141823-83-8
C₄₄H₅₇N₃O₁₃S

Guidance literature:: Multi-step reaction with 13 steps

1: AgClO₄, SnCl₂, molecular sieves (4 Angstroem) / tetrahydrofuran / 7 h / -78 - -20 °C

2: NaH / tetrahydrofuran; ethane-1,2-diol / 0.5 h / 25 °C

3: 1.) n-Bu₂SnO, 2.) n-Bu₃SnOMe, Br₂ / 1.) MeOH, reflux, 1.2 h, 2.) CH₂Cl₂, 25 deg C

4: 70 percent / pyridinium p-toluenesulfonate / benzene / 3 h / 25 °C

5: 100 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h / 0 to 25 deg C

6: 95 percent / i-Bu₂AlH / CH₂Cl₂ / 0.5 h / -78 °C

7: 86 percent / acetonitrile / 1.5 h / 25 °C

8: 100 percent / toluene / 1 h / 100 °C

9: 95 percent / NaSMe, EtSH / CH₂Cl₂ / 1.5 h / 25 °C

10: 90 percent / i-Pr₂EtN / CH₂Cl₂ / 1 h / 25 °C

11: 1.) AcOH, n-Bu₄NF, 2.) K-Selectride / 1.) THF, -40 to 0 deg C, 2.) DME, THF, -78 deg C, 0.7 h

12: 85 percent / HF*py / CH₂Cl₂; tetrahydrofuran / 3 h / -20 - 0 °C

13: NaBH₃CN, BF₃*OEt₂ / CH₂Cl₂; tetrahydrofuran; diethyl ether / 2 h / -60 - -40 °C

With 2,6-dimethylpyridine; 4 A molecular sieve; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; bromine; tributyltin methoxide; silver perchlorate; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; di(n-butyl)tin oxide; sodium cyanoborohydride; potassium tri-sec-butyl-borohydride; pyridine hydrogenfluoride; acetic acid; N-ethyl-N,N-diisopropylamine; ethanethiol; tin(ll) chloride; sodium thiomethoxide; In tetrahydrofuran; diethyl ether; dichloromethane; ethylene glycol; toluene; acetonitrile; benzene;