N-[(2,4-dichloro-3-methylphenyl)sulfonyl]-N-methyl-β-alanine ethyl ester

Base Information

Chemical Name:N-[(2,4-dichloro-3-methylphenyl)sulfonyl]-N-methyl-β-alanine ethyl ester
CAS No.:633696-62-5
Molecular Formula:C₁₃H₁₇Cl₂NO₄S
Molecular Weight:354.254
Hs Code.:

Synonyms:N-[(2,4-dichloro-3-methylphenyl)sulfonyl]-N-methyl-β-alanine ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(2,4-dichloro-3-methylphenyl)sulfonyl]-N-methyl-β-alanine ethyl ester

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Technology Process of N-[(2,4-dichloro-3-methylphenyl)sulfonyl]-N-methyl-β-alanine ethyl ester

There total 3 articles about N-[(2,4-dichloro-3-methylphenyl)sulfonyl]-N-methyl-β-alanine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 441295-86-9
N-methyl-2,4-dichloro-3-methylbenzenesufonamide

: 539-74-2
Ethyl 3-bromopropionate

: 633696-62-5
N-[(2,4-dichloro-3-methylphenyl)sulfonyl]-N-methyl-β-alanine ethyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 15h;
DOI:10.1021/jm2016057

Reference yield: 43.0%

: 633696-62-5
N-[(2,4-dichloro-3-methylphenyl)sulfonyl]-N-methyl-β-alanine ethyl ester

Guidance literature:

Reference yield:

: 69145-58-0
2,4-Dichloro-3-methylbenzenesulfonyl chloride

: 633696-62-5
N-[(2,4-dichloro-3-methylphenyl)sulfonyl]-N-methyl-β-alanine ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 15 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 15 h / 20 °C

With potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm2016057