1-phenyl-4-(phenylsilyl)butane

Base Information

• Chemical Name: 1-phenyl-4-(phenylsilyl)butane
• CAS No.: 1351520-69-8
• Molecular Formula: C₁₆H₂₀Si
• Molecular Weight: 240.42
• Mol file: 1351520-69-8.mol

Synonyms:1-phenyl-4-(phenylsilyl)butane

Chemical Property of 1-phenyl-4-(phenylsilyl)butane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1-phenyl-4-(phenylsilyl)butane

There total 7 articles about 1-phenyl-4-(phenylsilyl)butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-Phenylbut-1-ene (768-56-9) + phenylsilane (694-53-1) → 1-phenyl-4-(phenylsilyl)butane (1351520-69-8)

Guidance literature:

With C₆₆H₁₀₆N₄O₆Sm₂; In toluene; at 60 ℃; for 5h; regioselective reaction; Inert atmosphere; Glovebox; Schlenk technique;

DOI:10.1021/acs.inorgchem.6b01670

Reference yield: 90.0%

5-phenylpent-1-ene (1075-74-7) + phenylsilane (694-53-1) → 1-phenyl-4-(phenylsilyl)butane (1351520-69-8)

Guidance literature:

With C₅₆H₈₀N₄Si₄Yb₂; In toluene; at 70 ℃; for 6h; regioselective reaction; Catalytic behavior; Inert atmosphere; Schlenk technique;

DOI:10.1039/c7dt01837a

Reference yield: 72.0%

4-Phenylbut-1-ene (768-56-9) + phenylchlorosilane (4206-75-1) → 1-phenyl-4-(phenylsilyl)butane (1351520-69-8)

Guidance literature:

4-Phenylbut-1-ene; With iron(III) chloride; tributylphosphine; copper(I) bromide; In diethyl ether; at -20 ℃; for 0.0833333h; Inert atmosphere;

With cyclopentylmagnesium bromide; In diethyl ether; at -20 ℃; for 1h; Inert atmosphere;

phenylchlorosilane; In diethyl ether; at 30 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ja206745w

upstream raw materials:

4-Phenylbut-1-ene

phenylchlorosilane

phenylsilane

5-phenylpent-1-ene