1-(2-carboxyphenyl)-2-nitro-6,7-dimethoxy-3-methyl-3,4-dihydronaphthalene

Base Information

• Chemical Name: 1-(2-carboxyphenyl)-2-nitro-6,7-dimethoxy-3-methyl-3,4-dihydronaphthalene
• CAS No.: 1315172-44-1
• Molecular Formula: C₂₀H₁₉NO₆
• Molecular Weight: 369.374
• Mol file: 1315172-44-1.mol

Synonyms:1-(2-carboxyphenyl)-2-nitro-6,7-dimethoxy-3-methyl-3,4-dihydronaphthalene

Chemical Property of 1-(2-carboxyphenyl)-2-nitro-6,7-dimethoxy-3-methyl-3,4-dihydronaphthalene

Chemical Property:

Purity/Quality:

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Technology Process of 1-(2-carboxyphenyl)-2-nitro-6,7-dimethoxy-3-methyl-3,4-dihydronaphthalene

There total 1 articles about 1-(2-carboxyphenyl)-2-nitro-6,7-dimethoxy-3-methyl-3,4-dihydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.9%

C21H23NO7 (1315172-42-9) → 1-(2-carboxyphenyl)-2-nitro-6,7-dimethoxy-3-methyl-3,4-dihydronaphthalene (1315172-44-1)

Guidance literature:

C₂₁H₂₃NO₇; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; at 20 ℃; Inert atmosphere;

With hydrogenchloride; In water; pH=6;

DOI:10.1021/jm200334c

Reference yield:

1-(2-carboxyphenyl)-2-nitro-6,7-dimethoxy-3-methyl-3,4-dihydronaphthalene (1315172-44-1) → (+/-)-trans-1-(2-carboxyphenyl)-2-nitro-6,7-dimethoxy-3-methyl-3,4-dihydronaphthalene + (+/-)-trans-1-(2-carboxyphenyl)-2-nitro-6,7-dimethoxy-3-methyl-3,4-dihydronaphthalene

Guidance literature:

With sodium tetrahydroborate; In isopropyl alcohol; optical yield given as %de; Inert atmosphere; Reflux;

DOI:10.1021/jm200334c

upstream raw materials:

C₂₁H₂₃NO₇